Methanesulfonic acid, trifluoro-, 6-methoxy-1-[4-[2-(1-piperidinyl)ethoxy]phenoxy]-2-naphthalenyl ester

Base Information

Chemical Name:Methanesulfonic acid, trifluoro-, 6-methoxy-1-[4-[2-(1-piperidinyl)ethoxy]phenoxy]-2-naphthalenyl ester
CAS No.:648904-46-5
Molecular Formula:C25H26F3NO6S
Molecular Weight:525.546
Hs Code.:

Synonyms:trifluoro-methanesulfonic acid 6-methoxy-1-[4-(2-piperidin-1-yl-ethoxy)-phenoxy]-naphthalen-2-yl ester;trifluoromethanesulfonic acid 6-methoxy-1-[4-(2-piperidin-1-yl-ethoxy)-phenoxy]-naphthalen-2-yl ester;6-methoxy-1-(4-(2-(piperidin-1-yl)ethoxy)phenoxy)naphthalen-2-yl trifluoromethanesulfonate;

Suppliers and Price of Methanesulfonic acid, trifluoro-, 6-methoxy-1-[4-[2-(1-piperidinyl)ethoxy]phenoxy]-2-naphthalenyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Methanesulfonic acid, trifluoro-, 6-methoxy-1-[4-[2-(1-piperidinyl)ethoxy]phenoxy]-2-naphthalenyl ester

Chemical Property:

PSA：82.68000
LogP:6.75250

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Methanesulfonic acid, trifluoro-, 6-methoxy-1-[4-[2-(1-piperidinyl)ethoxy]phenoxy]-2-naphthalenyl ester

There total 7 articles about Methanesulfonic acid, trifluoro-, 6-methoxy-1-[4-[2-(1-piperidinyl)ethoxy]phenoxy]-2-naphthalenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 648904-49-8
6-methoxy-1-[4-(2-piperidin-1-ylethoxy)phenoxy]naphthalene-2-ol

: 358-23-6
trifluoromethylsulfonic anhydride

: 648904-46-5
trifluoromethanesulfonic acid 6-methoxy-1-[4-(2-piperidin-1-ylethoxy)phenoxy]naphthalen-2-yl ester

Guidance literature:: With triethylamine; In dichloromethane; at -50 - 20 ℃; for 3h;
DOI:10.1021/jm050723z

Reference yield: 90.9%

: 358-23-6
trifluoromethylsulfonic anhydride

: 648904-46-5
trifluoromethanesulfonic acid 6-methoxy-1-[4-(2-piperidin-1-ylethoxy)phenoxy]naphthalen-2-yl ester

Guidance literature:: 6-methoxy-1-[4-(2-piperidin-1-ylethoxy)phenoxy]naphthalene-2-ol; With triethylamine; In dichloromethane; at -50 ℃;

trifluoromethylsulfonic anhydride; at -50 - 20 ℃; for 3h;

Reference yield:

: 648904-47-6
2-(benzyloxy)-1-bromo-6-methoxynaphthalene

: 648904-46-5
trifluoromethanesulfonic acid 6-methoxy-1-[4-(2-piperidin-1-ylethoxy)phenoxy]naphthalen-2-yl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 30 percent / copper triflate

2: NH₄HCO₂ / Pd(OH)2

With ammonium formate; copper(I) triflate; palladium dihydroxide; 1: Ullman coupling;
DOI:10.1016/j.bmcl.2007.04.044