3,3-DIMETHYL-PIPERIDIN-4-ONE HCL SALT

Base Information

• Chemical Name: 3,3-DIMETHYL-PIPERIDIN-4-ONE HCL SALT
• CAS No.: 648921-37-3
• Molecular Formula: C7H13NO.ClH
• Molecular Weight: 163.647
• Hs Code.: 2933399990
• Mol file: 648921-37-3.mol

Synonyms:3,3-DIMETHYL-PIPERIDIN-4-ONE HCL SALT;3,3-dimethyl-4-oxopiperidium chloride;4-Piperidinone,3,3-dimethyl-,hydrochloride;3,3-DIMETHYLPIPERIDIN-4-ONE HYDROCHLORIDE;3,3-DIMETHYLPIPERIDIN-4-ONE HCL;

Chemical Property of 3,3-DIMETHYL-PIPERIDIN-4-ONE HCL SALT

Chemical Property:

• PSA: 29.10000
• LogP: 1.70580
• Storage Temp.: Inert atmosphere,Room Temperature

Purity/Quality:

97% ^*data from raw suppliers

3,3-Dimethylpiperidin-4-onehydrochloride ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3,3-DIMETHYL-PIPERIDIN-4-ONE HCL SALT

There total 2 articles about 3,3-DIMETHYL-PIPERIDIN-4-ONE HCL SALT which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.67%

N-benzyl-3,3-dimethylpiperidine-4-one (173186-91-9) → 3,3-dimethylpiperidin-4-one hydrochloride (648921-37-3)

Guidance literature:

N-benzyl-3,3-dimethylpiperidine-4-one; With carbonochloridic acid 1-chloro-ethyl ester; In 1,2-dichloro-ethane; at 80 ℃; for 12h;

With methanol; at 80 ℃; for 4h;

Reference yield: 78.0%

tert-butyl 3,3-dimethyl-4-oxopiperidine-1-carboxylate (324769-06-4) → 3,3-dimethylpiperidin-4-one hydrochloride (648921-37-3)

Guidance literature:

With hydrogenchloride; In tetrahydrofuran; at 20 - 60 ℃; for 3h;

Reference yield: 84.0%

3,3-dimethylpiperidin-4-one hydrochloride (648921-37-3) + 3-benzoylamino-3-methylbutanoic acid (17207-42-0) → N-(4-(3,3-dimethyl-4-oxopiperidin-1-yl)-2-methyl-4-oxobtutan-2-yl)benzamide (1108154-51-3)

Guidance literature:

With benzotriazol-1-ol; N-isopropylethylamine; In N,N-dimethyl-formamide; at 20 ℃;

upstream raw materials:

tert-butyl 3,3-dimethyl-4-oxopiperidine-1-carboxylate

N-benzyl-3,3-dimethylpiperidine-4-one

Downstream raw materials:

N-(4-(3,3-dimethyl-4-oxopiperidin-1-yl)-2-methyl-4-oxobtutan-2-yl)benzamide

C₁₅H₂₄N₂

3,3-dimethyl-1-tosylpiperidin-4-one

5-bromo-3,3-dimethyl-1-tosylpiperidin-4-one

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