[1,1'-Biphenyl]-2-amine, N-[(diphenylphosphino)diphenylphosphoranylidene]-

Base Information

Chemical Name:[1,1'-Biphenyl]-2-amine, N-[(diphenylphosphino)diphenylphosphoranylidene]-
CAS No.:648930-39-6
Molecular Formula:C36H29NP2
Molecular Weight:537.58
Hs Code.:

Synonyms:

Suppliers and Price of [1,1'-Biphenyl]-2-amine, N-[(diphenylphosphino)diphenylphosphoranylidene]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of [1,1'-Biphenyl]-2-amine, N-[(diphenylphosphino)diphenylphosphoranylidene]-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of [1,1'-Biphenyl]-2-amine, N-[(diphenylphosphino)diphenylphosphoranylidene]-

There total 1 articles about [1,1'-Biphenyl]-2-amine, N-[(diphenylphosphino)diphenylphosphoranylidene]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 90-41-5
2-phenylaniline

: 1079-66-9,74391-44-9
chloro-diphenylphosphine

: 648930-39-6
P(C₆H₅)2P(C₆H₅)2NC₆H₄C₆H₅

: C₃₆H₂₉NP₂

Guidance literature:: With triethylamine; In diethyl ether; at 20 ℃; for 168000h;
DOI:10.1039/b303645f

Reference yield: 75.0%

: 12107-56-1
dichloro(1,5-cyclooctadiene)palladium(II)

: 648930-39-6
P(C₆H₅)2P(C₆H₅)2NC₆H₄C₆H₅

: 898232-83-2
Pd(C₆H₄(o-Ph)N(PPh₂)2)Cl₂

Guidance literature:: In dichloromethane; (under N2, Schlenk); Pd-complex in CH2Cl2 added to soln. of ligand in CH2Cl2 at 0°C, warmed to room temp.; solvent removed under reduced pressure, THF or Et2O added, stored at 2°C for 24 h, filtered; elem. anal.;
DOI:10.1016/j.ica.2005.09.058

Reference yield: 61.0%

: 12080-32-9
dichloro( 1,5-cyclooctadiene)platinum(ll)

: 648930-39-6
P(C₆H₅)2P(C₆H₅)2NC₆H₄C₆H₅

: Pt(C₆H₄(o-Ph)N(PPh₂)2)2Cl₂

Guidance literature:: In dichloromethane; (under N2, Schlenk); Pt-complex in CH2Cl2 added to soln. of ligand in CH2Cl2 at 0°C, warmed to room temp., stirred for 4 h; solvent removed under reduced pressure, washed with Et2O, suspended in CH2Cl2 and Et2O, stored at -21°C for 1-2 d, filtered; elem. anal.;
DOI:10.1016/j.ica.2005.09.058