Methanesulfonic acid, trifluoro-, 3-hydroxy-4-(methoxyacetyl)phenyl ester

Base Information

Chemical Name:Methanesulfonic acid, trifluoro-, 3-hydroxy-4-(methoxyacetyl)phenyl ester
CAS No.:649551-91-7
Molecular Formula:C10H9F3O6S
Molecular Weight:314.239
Hs Code.:

Synonyms:1-(2'-hydroxy-4'-trifluoromethanesulfonyloxy)-phenyl-2-methoxy ethanone;

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Methanesulfonic acid, trifluoro-, 3-hydroxy-4-(methoxyacetyl)phenyl ester

Chemical Property:

PSA：98.28000
LogP:2.53050

Purity/Quality:

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Technology Process of Methanesulfonic acid, trifluoro-, 3-hydroxy-4-(methoxyacetyl)phenyl ester

There total 2 articles about Methanesulfonic acid, trifluoro-, 3-hydroxy-4-(methoxyacetyl)phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 108-46-3
recorcinol

: 649551-91-7
2'-hydroxy-2-methoxy-4'-trifluoromethanesulfonyloxy-acetophenone

Guidance literature:: Multi-step reaction with 2 steps

1.1: zinc chloride; hydrogen chloride / diethyl ether / 2 h

1.2: 48 percent / H₂O / 1 h / Heating

2.1: 2,6-lutidine / CH₂Cl₂ / 2 h

With 2,6-dimethylpyridine; hydrogenchloride; zinc(II) chloride; In diethyl ether; dichloromethane; 1.1: Houben-Hoesch reaction;
DOI:10.1016/j.bmc.2004.02.031

Reference yield:

: 358-23-6
trifluoromethylsulfonic anhydride

: 57280-75-8
2',4'-dihydroxy-2-methoxyacetophenone

: 649551-91-7
2'-hydroxy-2-methoxy-4'-trifluoromethanesulfonyloxy-acetophenone

: Trifluoro-methanesulfonic acid 2-(2-methoxy-acetyl)-5-trifluoromethanesulfonyloxy-phenyl ester

Guidance literature:: With 2,6-dimethylpyridine; In dichloromethane; for 2h;
DOI:10.1016/j.bmc.2004.02.031

Reference yield: 30.0%

: 872-05-9,17438-89-0,25189-70-2
1-Decene

: 649551-91-7
2'-hydroxy-2-methoxy-4'-trifluoromethanesulfonyloxy-acetophenone

: 649551-92-8
2'-hydroxy-4'-decyl-2-methoxy-acetophenone

Guidance literature:: 1-Decene; With 9-bora-bicyclo[3.3.1]nonane; In tetrahydrofuran; at 20 ℃; for 6h;

2'-hydroxy-2-methoxy-4'-trifluoromethanesulfonyloxy-acetophenone; With potassium phosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; at 65 ℃; Heating / reflux;