phenyl dichloroacetate

Base Information

• Chemical Name: phenyl dichloroacetate
• CAS No.: 10565-20-5
• Molecular Formula: C8H6Cl2O2
• Molecular Weight: 205.04
• Mol file: 10565-20-5.mol

Synonyms:

Chemical Property of phenyl dichloroacetate

Chemical Property:

• Vapor Pressure: 0.0265mmHg at 25°C
• Boiling Point: 246.9°Cat760mmHg
• Flash Point: 102.4°C
• Density: 1.365g/cm³

Purity/Quality:

97% purity ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of phenyl dichloroacetate

There total 7 articles about phenyl dichloroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

dichloroacethyl chloride (79-36-7) + phenol (108-95-2,27073-41-2) → phenyl dichloroacetate (10565-20-5)

Guidance literature:

With 1,1,1,3,3-pentafluoro-2,3-dichloropropane; at 60 - 80 ℃; for 9h;

Reference yield: 65.0%

trichloroethylene epoxide (16967-79-6) + phenol (108-95-2,27073-41-2) → phenyl dichloroacetate (10565-20-5) + phenyl phenoxychloroacetate (87148-44-5)

Guidance literature:

With magnesium sulfate; at 100 ℃; for 1h;

Reference yield: 56.0%

phenyl trichloroacetate (10112-13-7) → phenyl dichloroacetate (10565-20-5)

Guidance literature:

With palladium 10% on activated carbon; hydrogen; In N,N-dimethyl acetamide; at 25 ℃; for 0.8h; under 760.051 Torr; chemoselective reaction;

DOI:10.1002/adsc.201100778

upstream raw materials:

(E)-1,2-dichloro-1-ethoxy-ethene

dichloroacethyl chloride

phenol

dichloroacetic anhydride

Downstream raw materials:

dichloro-acetic acid-(1,2,3,4,5,6-hexachloro-cyclohexyl ester)

dichloro-acetic acid

phenol

(E)-but-2-enedioic acid diphenyl ester