Acetic acid, 2,2'-[[4-[[5-methoxy-2-[[(4-methoxy-3,5-dimethyl-2-pyridinyl)methyl]sulfin yl]-1H-benzimidazol-1-yl]sulfonyl]-1,2-phenylene]bis(oxy)]bis-, bis[2-[(4-methylphenyl)sulfonyl]ethyl] ester

Base Information

• Chemical Name: Acetic acid, 2,2'-[[4-[[5-methoxy-2-[[(4-methoxy-3,5-dimethyl-2-pyridinyl)methyl]sulfin yl]-1H-benzimidazol-1-yl]sulfonyl]-1,2-phenylene]bis(oxy)]bis-, bis[2-[(4-methylphenyl)sulfonyl]ethyl] ester
• CAS No.: 651728-64-2
• Molecular Formula: C45H47N3O15S4
• Molecular Weight: 998.143

Synonyms:

Chemical Property of Acetic acid, 2,2'-[[4-[[5-methoxy-2-[[(4-methoxy-3,5-dimethyl-2-pyridinyl)methyl]sulfin yl]-1H-benzimidazol-1-yl]sulfonyl]-1,2-phenylene]bis(oxy)]bis-, bis[2-[(4-methylphenyl)sulfonyl]ethyl] ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Acetic acid, 2,2'-[[4-[[5-methoxy-2-[[(4-methoxy-3,5-dimethyl-2-pyridinyl)methyl]sulfin yl]-1H-benzimidazol-1-yl]sulfonyl]-1,2-phenylene]bis(oxy)]bis-, bis[2-[(4-methylphenyl)sulfonyl]ethyl] ester

There total 2 articles about Acetic acid, 2,2'-[[4-[[5-methoxy-2-[[(4-methoxy-3,5-dimethyl-2-pyridinyl)methyl]sulfin yl]-1H-benzimidazol-1-yl]sulfonyl]-1,2-phenylene]bis(oxy)]bis-, bis[2-[(4-methylphenyl)sulfonyl]ethyl] ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

2-(4-tolylsulfonyl)ethyl 4-[(5-methoxy-([4-methoxy-3,5-dimethyl(2-pyridyl)]methylthio)-benzimidazolyl)sulfonyl]-2-(2-[4-tolylsulfonyl]ethoxycarbonylmethoxy)phenoxyacetate (651729-57-6) → {4-[5-methoxy-2-(4-methoxy-3,5-dimethylpyridin-2-ylmethanesulfinyl)benzimidazole-1-sulfonyl]-2-[2-(toluene-4-sulfonyl)ethoxycarbonylmethoxy]phenoxy}acetic acid 2-(toluene-4-sulfonyl)ethyl ester (651728-64-2)

Guidance literature:

With m-chloroperoxybenzoic acid; In tetrahydrofuran; for 17.1667h;

Reference yield:

{4-chlorosulfonyl-2-[2-(toluene-4-sulfonyl)ethoxycarbonylmethoxy]-phenoxy}acetic acid 2-(toluene-4-sulfonyl)ethyl ester (651728-63-1) + omeprazole (73590-58-6) → {4-[5-methoxy-2-(4-methoxy-3,5-dimethylpyridin-2-ylmethanesulfinyl)benzimidazole-1-sulfonyl]-2-[2-(toluene-4-sulfonyl)ethoxycarbonylmethoxy]phenoxy}acetic acid 2-(toluene-4-sulfonyl)ethyl ester (651728-64-2) + {4-[6-methoxy-2-(4-methoxy-3,5-dimethylpyridin-2-ylmethanesulfinyl)benzimidazole-1-sulfonyl]-2-[2-(toluene-4-sulfonyl)ethoxycarbonylmethoxy]phenoxy}acetic acid 2-(toluene-4-sulfonyl)ethyl ester (651728-65-3)

Guidance literature:

With triethylamine; In dichloromethane; at 20 ℃; for 6h;

Reference yield: 49.0%

{4-[5-methoxy-2-(4-methoxy-3,5-dimethylpyridin-2-ylmethanesulfinyl)benzimidazole-1-sulfonyl]-2-[2-(toluene-4-sulfonyl)ethoxycarbonylmethoxy]phenoxy}acetic acid 2-(toluene-4-sulfonyl)ethyl ester (651728-64-2) → {2-carboxymethoxy-4-[5-methoxy-2-(4-methoxy-3,5-dimethylpyridin-2-ylmethanesulfinyl)benzimidazole-1-sulfonyl]phenoxy}acetic acid disodium salt

Guidance literature:

With sodium hydrogencarbonate; In water; isopropyl alcohol; acetonitrile; at 70 ℃; for 1.25h;

upstream raw materials:

{4-chlorosulfonyl-2-[2-(toluene-4-sulfonyl)ethoxycarbonylmethoxy]-phenoxy}acetic acid 2-(toluene-4-sulfonyl)ethyl ester

omeprazole

2-(4-tolylsulfonyl)ethyl 4-[(5-methoxy-([4-methoxy-3,5-dimethyl(2-pyridyl)]methylthio)-benzimidazolyl)sulfonyl]-2-(2-[4-tolylsulfonyl]ethoxycarbonylmethoxy)phenoxyacetate

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