Phosphinic acid, [(phenylmethoxy)methyl]-, ethyl ester

Base Information

Chemical Name:Phosphinic acid, [(phenylmethoxy)methyl]-, ethyl ester
CAS No.:653585-12-7
Molecular Formula:C10H15O3P
Molecular Weight:214.201
Hs Code.:
DSSTox Substance ID:DTXSID90459083
Wikidata:Q82282690

Synonyms:Phosphinic acid, [(phenylmethoxy)methyl]-, ethyl ester;653585-12-7;DTXSID90459083

Suppliers and Price of Phosphinic acid, [(phenylmethoxy)methyl]-, ethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of Phosphinic acid, [(phenylmethoxy)methyl]-, ethyl ester

Chemical Property:

XLogP3:1.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:6
Exact Mass:213.06805630
Heavy Atom Count:14
Complexity:167

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CCO[P+](=O)COCC1=CC=CC=C1

Technology Process of Phosphinic acid, [(phenylmethoxy)methyl]-, ethyl ester

There total 2 articles about Phosphinic acid, [(phenylmethoxy)methyl]-, ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 78-10-4
tetraethoxy orthosilicate

: 674789-16-3
benzyloxymethyl-hydrogenphosphinic acid

: 653585-12-7
ethyl benzyloxymethyl-hydrogenphosphinate

Guidance literature:: In toluene; for 12h; Heating;
DOI:10.1055/s-2003-41045

Reference yield:

: 3587-60-8
Benzyloxymethyl chloride

: 653585-12-7
ethyl benzyloxymethyl-hydrogenphosphinate

Guidance literature:: Multi-step reaction with 2 steps

1: 3.63 g / bis(trimethylsilyl)phosphonite / CH₂Cl₂ / 0 - 20 °C

2: toluene / 12 h / Heating

With bis(trimethylsilyl) phosphonate; In dichloromethane; toluene;
DOI:10.1016/j.tet.2003.11.045