4-{(E)-[4-(dimethylamino)phenyl]diazenyl}benzoyl chloride

Base Information

• Chemical Name: 4-{(E)-[4-(dimethylamino)phenyl]diazenyl}benzoyl chloride
• CAS No.: 27128-58-1
• Molecular Formula: C₁₅H₁₄ClN₃O
• Molecular Weight: 287.749
• Mol file: 27128-58-1.mol

Synonyms:Benzoylchloride, 4-[[4-(dimethylamino)phenyl]azo]- (9CI); Benzoyl chloride,p-[[p-(dimethylamino)phenyl]azo]- (8CI); 4-Dimethylaminobenzene-4'-azobenzoylchloride; Dabcyl chloride; N,N-Dimethyl-p-aminobenzeneazobenzoyl chloride; NSC240870; p-(N,N-Dimethylamino)-p'-azobenzoyl chloride

Chemical Property of 4-{(E)-[4-(dimethylamino)phenyl]diazenyl}benzoyl chloride

Chemical Property:

• Vapor Pressure: 5.59E-08mmHg at 25°C
• Boiling Point: 441.1°Cat760mmHg
• Flash Point: 220.6°C
• Density: 1.18g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-{(E)-[4-(dimethylamino)phenyl]diazenyl}benzoyl chloride

There total 1 articles about 4-{(E)-[4-(dimethylamino)phenyl]diazenyl}benzoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

p-methyl red (201858-51-7) → N,N-dimethyl-p-aminophenylazobenzoyl chloride (27128-58-1)

Guidance literature:

With thionyl chloride; In dichloromethane; Reflux;

DOI:10.1002/chem.200901607

Reference yield:

N,N-dimethyl-p-aminophenylazobenzoyl chloride (27128-58-1) → 4-(4-dimethylaminophenylazo)benzoyl fluoride (1082488-99-0)

Guidance literature:

With 2-[(CH₃)2NCH₂](C₆H₄)(n-Bu)2SnF; In benzene; at 20 ℃; for 1h; Inert atmosphere;

DOI:10.1016/j.tetlet.2008.08.060

Reference yield:

N,N-dimethyl-p-aminophenylazobenzoyl chloride (27128-58-1) + N,N-dimethylethylenediamine (108-00-9) → C19H25N5O (1262997-12-5)

Guidance literature:

In dichloromethane; at 0 - 20 ℃;

DOI:10.1002/chem.200901607

upstream raw materials:

p-methyl red

Downstream raw materials:

4-(4-dimethylaminophenylazo)benzoyl fluoride

C₁₉H₂₅N₅O