N-BOC-4-broMo-3-Methylaniline

Base Information

Chemical Name:N-BOC-4-broMo-3-Methylaniline
CAS No.:654056-82-3
Molecular Formula:C12H16BrNO2
Molecular Weight:286.16500
Hs Code.:2924299090
Mol file:654056-82-3.mol

Synonyms:N-BOC-4-bromo-3-methylaniline;Carbamic acid,(4-bromo-3-methylphenyl)-,1,1-dimethylethyl ester;

Suppliers and Price of N-BOC-4-broMo-3-Methylaniline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
N-BOC-4-bromo-3-methylaniline
100mg
$ 45.00

TRC
N-BOC-4-bromo-3-methylaniline
500mg
$ 115.00

Crysdot
N-BOC-4-bromo-3-methylaniline 95+%
25g
$ 594.00

Crysdot
N-BOC-4-bromo-3-methylaniline 95+%
10g
$ 297.00

Chemcia Scientific
(4-Bromo-3-methyl-phenyl)-carbamicacidtert-butylester 95%
5 G
$ 295.00

AOBChem
Tert-butyl(4-bromo-3-methylphenyl)carbamate 97%
10g
$ 316.00

Ambeed
N-BOC-4-bromo-3-methylaniline 95%
5g
$ 178.00

Ambeed
N-BOC-4-bromo-3-methylaniline 95%
25g
$ 578.00

Ambeed
N-BOC-4-bromo-3-methylaniline 95%
1g
$ 52.00

Ambeed
N-BOC-4-bromo-3-methylaniline 95%
250mg
$ 21.00

Total 9 raw suppliers

Chemical Property of N-BOC-4-broMo-3-Methylaniline

Chemical Property:

Boiling Point:297.3±33.0 °C(Predicted)
PKA:12.99±0.70(Predicted)
PSA：38.33000
Density:1.356±0.06 g/cm3(Predicted)
LogP:4.17750
Storage Temp.:2-8°C

Purity/Quality:

97% ^*data from raw suppliers

N-BOC-4-bromo-3-methylaniline ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of N-BOC-4-broMo-3-Methylaniline

There total 2 articles about N-BOC-4-broMo-3-Methylaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 6933-10-4
amino-5-bromo-2-toluene

: 654056-82-3
(4-bromo-3-methylphenyl)carbamic acid tert-butyl ester

Guidance literature:: With indium(III) bromide; at 30 - 35 ℃; for 0.5h;
DOI:10.1055/s-2006-942492

Reference yield: 100.0%

: 1591-97-5
4-bromo-3-methylphenyl isocyanate

: 75-65-0
tert-butyl alcohol

: 654056-82-3
(4-bromo-3-methylphenyl)carbamic acid tert-butyl ester

Guidance literature:: at 80 ℃; for 16h; Inert atmosphere;
DOI:10.1021/acs.orglett.5b03061

Reference yield:

: 654056-82-3
(4-bromo-3-methylphenyl)carbamic acid tert-butyl ester

: 25487-66-5
3-Carboxyphenylboronic acid

: 929890-98-2
4'-tert-butoxycarbonylamino-2'-methyl-biphenyl-3-carboxylic acid

Guidance literature:: With caesium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,2-dimethoxyethane; water; for 18h; Heating / reflux;