Benzenesulfonamide, N-(3-iodopropyl)-4-methyl-N-(2-oxoethyl)-

Base Information

Chemical Name:Benzenesulfonamide, N-(3-iodopropyl)-4-methyl-N-(2-oxoethyl)-
CAS No.:654673-69-5
Molecular Formula:C12H16INO3S
Molecular Weight:381.234
Hs Code.:
DSSTox Substance ID:DTXSID00462124
Nikkaji Number:J1.999.527E
Wikidata:Q82286621

Synonyms:654673-69-5;Benzenesulfonamide, N-(3-iodopropyl)-4-methyl-N-(2-oxoethyl)-;DTXSID00462124

Suppliers and Price of Benzenesulfonamide, N-(3-iodopropyl)-4-methyl-N-(2-oxoethyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of Benzenesulfonamide, N-(3-iodopropyl)-4-methyl-N-(2-oxoethyl)-

Chemical Property:

XLogP3:2.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:7
Exact Mass:380.98956
Heavy Atom Count:18
Complexity:345

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=C(C=C1)S(=O)(=O)N(CCCI)CC=O

Technology Process of Benzenesulfonamide, N-(3-iodopropyl)-4-methyl-N-(2-oxoethyl)-

There total 3 articles about Benzenesulfonamide, N-(3-iodopropyl)-4-methyl-N-(2-oxoethyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 654673-64-0
N-(2,2-dimethoxyethyl)-N-(3-iodopropyl)-4-methylbenzenesulfonamide

: 654673-69-5
N-(3-iodopropyl)-4-methyl-N-(2-oxoethyl)benzenesulfonamide

Guidance literature:: With hydrogenchloride; In water; acetone; at 20 ℃; for 48h;
DOI:10.1039/c3cc45452e

Reference yield:

: 58754-95-3
N-(2,2-dimethoxyethyl)-p-toluenesulfonamide

: 654673-69-5
N-(3-iodopropyl)-4-methyl-N-(2-oxoethyl)benzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: NaH / tetrahydrofuran / 0 - 20 °C

1.2: 65 percent / tetrahydrofuran / 36 h / Heating

2.1: 53 percent / aq. HCl / acetone / 48 h

With hydrogenchloride; sodium hydride; In tetrahydrofuran; acetone;
DOI:10.1021/ja0392566

Reference yield:

: 98-59-9
p-toluenesulfonyl chloride

: 654673-69-5
N-(3-iodopropyl)-4-methyl-N-(2-oxoethyl)benzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: 82 percent / triethylamine / CH₂Cl₂ / 24 h

2.1: NaH / tetrahydrofuran / 0 - 20 °C

2.2: 65 percent / tetrahydrofuran / 36 h / Heating

3.1: 53 percent / aq. HCl / acetone / 48 h

With hydrogenchloride; sodium hydride; triethylamine; In tetrahydrofuran; dichloromethane; acetone;
DOI:10.1021/ja0392566