(S)-N-(3-iodopropyl)-N-(2-((mesitylsulfinyl)imino)ethyl)-4-methylbenzenesulfonamide

Base Information

Chemical Name:(S)-N-(3-iodopropyl)-N-(2-((mesitylsulfinyl)imino)ethyl)-4-methylbenzenesulfonamide
CAS No.:1459793-12-4
Molecular Formula:C₂₁H₂₇IN₂O₃S₂
Molecular Weight:546.493
Hs Code.:

Synonyms:(S)-N-(3-iodopropyl)-N-(2-((mesitylsulfinyl)imino)ethyl)-4-methylbenzenesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-N-(3-iodopropyl)-N-(2-((mesitylsulfinyl)imino)ethyl)-4-methylbenzenesulfonamide

Chemical Property:

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Technology Process of (S)-N-(3-iodopropyl)-N-(2-((mesitylsulfinyl)imino)ethyl)-4-methylbenzenesulfonamide

There total 3 articles about (S)-N-(3-iodopropyl)-N-(2-((mesitylsulfinyl)imino)ethyl)-4-methylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 607729-50-0
(S)-(+)-2,4,6-trimethylbenzenesulfinamide

: 654673-69-5
N-(3-iodopropyl)-4-methyl-N-(2-oxoethyl)benzenesulfonamide

: 1459793-12-4
(S)-N-(3-iodopropyl)-N-(2-((mesitylsulfinyl)imino)ethyl)-4-methylbenzenesulfonamide

Guidance literature:: With titanium(IV) tetraethanolate; In tetrahydrofuran; at 20 ℃; Inert atmosphere;
DOI:10.1039/c3cc45452e

Reference yield:

: 58754-95-3
N-(2,2-dimethoxyethyl)-p-toluenesulfonamide

: 1459793-12-4
(S)-N-(3-iodopropyl)-N-(2-((mesitylsulfinyl)imino)ethyl)-4-methylbenzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 0.17 h / 0 - 20 °C / Inert atmosphere

1.2: 19 h / Reflux; Inert atmosphere

2.1: hydrogenchloride / acetone; water / 48 h / 20 °C

3.1: titanium(IV) tetraethanolate / tetrahydrofuran / 20 °C / Inert atmosphere

With hydrogenchloride; titanium(IV) tetraethanolate; sodium hydride; In tetrahydrofuran; water; acetone; mineral oil;
DOI:10.1039/c3cc45452e

Reference yield:

: 654673-64-0
N-(2,2-dimethoxyethyl)-N-(3-iodopropyl)-4-methylbenzenesulfonamide

: 1459793-12-4
(S)-N-(3-iodopropyl)-N-(2-((mesitylsulfinyl)imino)ethyl)-4-methylbenzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride / acetone; water / 48 h / 20 °C

2: titanium(IV) tetraethanolate / tetrahydrofuran / 20 °C / Inert atmosphere

With hydrogenchloride; titanium(IV) tetraethanolate; In tetrahydrofuran; water; acetone;
DOI:10.1039/c3cc45452e