1,1',1''-[Benzene-1,3,5-triyltri(ethene-2,1-diyl)]tribenzene

Base Information

Chemical Name:1,1',1''-[Benzene-1,3,5-triyltri(ethene-2,1-diyl)]tribenzene
CAS No.:6566-16-1
Molecular Formula:C₃₀H₂₄
Molecular Weight:384.521
Hs Code.:
DSSTox Substance ID:DTXSID40709666

Synonyms:6566-16-1;DTXSID40709666;1,3,5-tris(phenylethenyl)benzene;1,1',1''-[Benzene-1,3,5-triyltri(ethene-2,1-diyl)]tribenzene

Suppliers and Price of 1,1',1''-[Benzene-1,3,5-triyltri(ethene-2,1-diyl)]tribenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 1,1',1''-[Benzene-1,3,5-triyltri(ethene-2,1-diyl)]tribenzene

Chemical Property:

XLogP3:9.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:6
Exact Mass:384.187800766
Heavy Atom Count:30
Complexity:456

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)C=CC2=CC(=CC(=C2)C=CC3=CC=CC=C3)C=CC4=CC=CC=C4

Technology Process of 1,1',1''-[Benzene-1,3,5-triyltri(ethene-2,1-diyl)]tribenzene

There total 5 articles about 1,1',1''-[Benzene-1,3,5-triyltri(ethene-2,1-diyl)]tribenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6
styrene

: 626-39-1
1,3,5-trisbromobenzene

: 34631-15-7,6566-16-1
1,3,5-tristyrylbenzene

Guidance literature:: With palladium diacetate; potassium carbonate; 1-[phenyl(piperidin-1-yl)methyl]naphthalen-2-ol; In N,N-dimethyl acetamide; at 60 - 140 ℃; Inert atmosphere; Sonication;
DOI:10.1080/00397911.2010.544439

Reference yield: 48.0%

: 100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6
styrene

: 34631-15-7,6566-16-1
1,3,5-tristyrylbenzene

Guidance literature:: With potassium carbonate; In N,N-dimethyl acetamide; at 65 - 140 ℃; for 40h; Inert atmosphere;
DOI:10.1002/aoc.3234

Reference yield:

: 100-52-7
benzaldehyde

: 34631-15-7,6566-16-1
1,3,5-tristyrylbenzene

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl acetamide / 60 °C / Inert atmosphere

2: potassium carbonate / N,N-dimethyl acetamide / 40 h / 65 - 140 °C / Inert atmosphere

With potassium carbonate; In N,N-dimethyl acetamide; 1: |Wittig Olefination / 2: |Heck Reaction;
DOI:10.1002/aoc.3234