Lauraldehyde 2,4-dinitrophenylhydrazone

Base Information

• Chemical Name: Lauraldehyde 2,4-dinitrophenylhydrazone
• CAS No.: 1726-78-9
• Molecular Formula: C18H28 N4 O4
• Molecular Weight: 364.445
• NSC Number: 405570
• DSSTox Substance ID: DTXSID00417735
• Mol file: 1726-78-9.mol

Synonyms:1726-78-9;AC1Q1ZLT;DTXSID00417735;ZSFFFYIXMCLEBX-XMHGGMMESA-N;NSC405570;Lauraldehyde 2,4-dinitrophenylhydrazone;NSC-405570;(1E)-Dodecanal (2,4-dinitrophenyl)hydrazone #

Chemical Property of Lauraldehyde 2,4-dinitrophenylhydrazone

Chemical Property:

• Vapor Pressure: 7.26E-10mmHg at 25°C
• Boiling Point: 493.1°C at 760 mmHg
• Flash Point: 252°C
• Density: 1.16g/cm³
• XLogP3: 6
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 6
• Rotatable Bond Count: 12
• Exact Mass: 364.21105539
• Heavy Atom Count: 26
• Complexity: 434

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCCCCCCCCCCC=NNC1=C(C=C(C=C1)[N+](=O)[O-])[N+](=O)[O-]
• Isomeric SMILES: CCCCCCCCCCC/C=N/NC1=C(C=C(C=C1)[N+](=O)[O-])[N+](=O)[O-]

Technology Process of Lauraldehyde 2,4-dinitrophenylhydrazone

There total 13 articles about Lauraldehyde 2,4-dinitrophenylhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Dodecanal (112-54-9) + (2,4-dinitro-phenyl)-hydrazine (119-26-6) → dodecanal (2,4-dinitrophenyl)hydrazone (1726-78-9)

Guidance literature:

DOI:10.1021/ja01176a082 DOI:10.1021/ja01867a068

Reference yield:

n-Dodecylamine (124-22-1) → dodecanal (2,4-dinitrophenyl)hydrazone (1726-78-9)

Guidance literature:

Multi-step reaction with 3 steps

1: 3,4-disubstituted 4-deazatoxoflavin derivative / 10 h / 120 °C

2: 2N HCl / diethyl ether

3: 2N HCl / diethyl ether

With hydrogenchloride; 3,4-disubstituted 4-deazatoxoflavin derivative; In diethyl ether;

DOI:10.1246/cl.1982.1309

Reference yield:

1-chloro-2,4-dinitro-benzene (97-00-7) → dodecanal (2,4-dinitrophenyl)hydrazone (1726-78-9)

Guidance literature:

Multi-step reaction with 2 steps

1: diluted alcohol

With ethanol;

upstream raw materials:

Dodecanal

(2,4-dinitro-phenyl)-hydrazine

(1-hydroxy-dodecyl)-phosphonic acid di-sec-butyl ester

1,1-diethoxy-dodeca-2c,6c-diene