1-Fluoro-1,1-dimethyl-N-(2,4,6-trimethylphenyl)silanamine

Base Information

• Chemical Name: 1-Fluoro-1,1-dimethyl-N-(2,4,6-trimethylphenyl)silanamine
• CAS No.: 65768-31-2
• Molecular Formula: C₁₁H₁₈FNSi
• Molecular Weight: 211.355
• DSSTox Substance ID: DTXSID40497076
• Wikidata: Q82346426

Synonyms:65768-31-2;DTXSID40497076;1-Fluoro-1,1-dimethyl-N-(2,4,6-trimethylphenyl)silanamine

Chemical Property of 1-Fluoro-1,1-dimethyl-N-(2,4,6-trimethylphenyl)silanamine

Chemical Property:

• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 2
• Exact Mass: 211.11925427
• Heavy Atom Count: 14
• Complexity: 184

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1=CC(=C(C(=C1)C)N[Si](C)(C)F)C

Technology Process of 1-Fluoro-1,1-dimethyl-N-(2,4,6-trimethylphenyl)silanamine

There total 1 articles about 1-Fluoro-1,1-dimethyl-N-(2,4,6-trimethylphenyl)silanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

dimethyldifluorosilane (353-66-2) + lithium 2,4,6-trimethylaniline (65768-38-9) → N-(Fluordimethylsilyl)-2,4-6-trimethylanilin (65768-31-2)

Guidance literature:

DOI:10.1007/BF00913009 DOI:10.1016/S0022-328X(00)84096-6

Reference yield:

N-(Fluordimethylsilyl)-2,4-6-trimethylanilin (65768-31-2) → 1-tert-Butyl-2-fluoro-2,4,4-trimethyl-3-(2,4,6-trimethyl-phenyl)-[1,3,2,4]diazadisiletidine (68913-89-3)

Guidance literature:

Multi-step reaction with 2 steps

1: (i) nBuLi, (ii) /BRN= 1732819/

DOI:10.1007/BF00913009

Reference yield:

methyltrifluorosilane (373-74-0) + N-(Fluordimethylsilyl)-2,4-6-trimethylanilin (65768-31-2) → 1,1,3-Trifluoro-1,3,3-trimethyl-2-(2,4,6-trimethyl-phenyl)-disilazane (68728-96-1)

Guidance literature:

Multistep reaction; (i) nBuLi, (ii) /BRN= 1732819/;

DOI:10.1007/BF00913009

upstream raw materials:

dimethyldifluorosilane

lithium 2,4,6-trimethylaniline

Downstream raw materials:

1,1,3-Trifluoro-1,3,3-trimethyl-2-(2,4,6-trimethyl-phenyl)-disilazane

1-tert-Butyl-2-fluoro-2,4,4-trimethyl-3-(2,4,6-trimethyl-phenyl)-[1,3,2,4]diazadisiletidine

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