(3beta,5beta,8xi,9xi)-5,14-dihydroxy-19-oxo-3-(beta-D-glycero-pentopyranosyloxy)card-20(22)-enolide

Base Information

Chemical Name:(3beta,5beta,8xi,9xi)-5,14-dihydroxy-19-oxo-3-(beta-D-glycero-pentopyranosyloxy)card-20(22)-enolide
CAS No.:15596-26-6
Molecular Formula:C₂₈H₄₀O₁₀
Molecular Weight:536.62
Hs Code.:
Mol file:15596-26-6.mol

Synonyms:5b-Card-20(22)-enolide,5,14-dihydroxy-19-oxo-3b-(b-D-xylopyranosyloxy)- (8CI); 3-O-b-D-Xylopyranosylstrophanthidin

Suppliers and Price of (3beta,5beta,8xi,9xi)-5,14-dihydroxy-19-oxo-3-(beta-D-glycero-pentopyranosyloxy)card-20(22)-enolide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3beta,5beta,8xi,9xi)-5,14-dihydroxy-19-oxo-3-(beta-D-glycero-pentopyranosyloxy)card-20(22)-enolide

Chemical Property:

Vapor Pressure:1.62E-26mmHg at 25°C
Boiling Point:757.9°Cat760mmHg
Flash Point:249.9°C
Density:1.44g/cm³

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of (3beta,5beta,8xi,9xi)-5,14-dihydroxy-19-oxo-3-(beta-D-glycero-pentopyranosyloxy)card-20(22)-enolide

There total 9 articles about (3beta,5beta,8xi,9xi)-5,14-dihydroxy-19-oxo-3-(beta-D-glycero-pentopyranosyloxy)card-20(22)-enolide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5,14-dihydroxy-19-oxo-3β-(tri-O-acetyl-α-L-arabinopyranosyloxy)-5β,14β-card-20(22)-enolide

: 15596-26-6,25486-24-2,28071-51-4,29505-40-6,86820-22-6
3β-α-L-arabinopyranosyloxy-5,14-dihydroxy-19-oxo-5β,14β-card-20(22)-enolide

Guidance literature:: With methanol; barium methoxide;
DOI:10.1021/jo01190a007

Reference yield:

: 5,14-dihydroxy-19-oxo-3β-(tri-O-acetyl-β-D-xylopyranosyloxy)-5β,14β-card-20(22)-enolide

: 15596-26-6,25486-24-2,28071-51-4,29505-40-6,86820-22-6
3-O-β-D-xylopyranosylstrophanthidin

Guidance literature:: With methanol; barium methoxide;
DOI:10.1021/jo01190a007

Reference yield:

: 14227-90-8
2,3,4-tri-O-acetyl-α-L-arabinopyranosyl bromide

: 15596-26-6,25486-24-2,28071-51-4,29505-40-6,86820-22-6
3β-α-L-arabinopyranosyloxy-5,14-dihydroxy-19-oxo-5β,14β-card-20(22)-enolide

Guidance literature:: Multi-step reaction with 2 steps

1: silver carbonate; magnesium sulfate; dioxane

2: ammonia; methanol

With 1,4-dioxane; methanol; ammonia; magnesium sulfate; silver carbonate;
DOI:10.1021/jo01190a007