Phenol, 3-[2-(4-nitrophenyl)ethenyl]-

Base Information

Chemical Name:Phenol, 3-[2-(4-nitrophenyl)ethenyl]-
CAS No.:65819-31-0
Molecular Formula:C₁₄H₁₁NO₃
Molecular Weight:241.246
Hs Code.:

Synonyms:

Suppliers and Price of Phenol, 3-[2-(4-nitrophenyl)ethenyl]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of Phenol, 3-[2-(4-nitrophenyl)ethenyl]-

Chemical Property:

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Phenol, 3-[2-(4-nitrophenyl)ethenyl]-

There total 3 articles about Phenol, 3-[2-(4-nitrophenyl)ethenyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 104-03-0
4-nitrobenzeneacetic acid

: 100-83-4
meta-hydroxybenzaldehyde

: 65819-31-0
4'-nitro-3-oxy-stilbene

Guidance literature:: With piperidine; at 110 ℃;

Reference yield:

: 100-11-8
1-bromomethyl-4-nitro-benzene

: 65819-31-0
4'-nitro-3-oxy-stilbene

Guidance literature:: Multi-step reaction with 2 steps

1: 3 h / 100 °C

2: 1.) 4-(hydroxymethyl)phenoxyacetic acid, HOBt, DIPCDI, (aminomethyl)polystyrene, 2.) CBr₄, PPh₃, 3.) <(CH₃)3SiNK, 4.) NaOMe, 5.) TFA / 1.) CH₂Cl₂, DMF, overnight, 2.) CH₂Cl₂, 0 deg C, 3.) DMF, overnight, 4.) DMF, overnight, 5.) H₂O, 2 h

With (aminomethyl)polystyrene; carbon tetrabromide; 1,3-di-tert-butylcarbodiimide; sodium methylate; potassium hexamethylsilazane; benzotriazol-1-ol; [4-(hydroxymethyl)phenoxy]acetic acid; triphenylphosphine; trifluoroacetic acid;
DOI:10.1021/jo9802269

Reference yield:

: 2609-49-6
diethyl p-nitrobenzylphosphonate

: 100-83-4
meta-hydroxybenzaldehyde

: 65819-31-0
4'-nitro-3-oxy-stilbene

Guidance literature:: With (aminomethyl)polystyrene; carbon tetrabromide; 1,3-di-tert-butylcarbodiimide; sodium methylate; potassium hexamethylsilazane; benzotriazol-1-ol; [4-(hydroxymethyl)phenoxy]acetic acid; triphenylphosphine; trifluoroacetic acid; Yield given. Multistep reaction; 1.) CH₂Cl₂, DMF, overnight, 2.) CH₂Cl₂, 0 deg C, 3.) DMF, overnight, 4.) DMF, overnight, 5.) H₂O, 2 h;
DOI:10.1021/jo9802269