AKOS 91597

Base Information

Chemical Name:AKOS 91597
CAS No.:658-24-2
Molecular Formula:C6H12N2
Molecular Weight:112.17300
Hs Code.:2933990090
Mol file:658-24-2.mol

Synonyms:2,5-DIAZA-BICYCLO[2.2.2]OCTANE;2,5-Diaza-bicyclo<2.2.2>octan;

Suppliers and Price of AKOS 91597

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

J&W Pharmlab
2,5-Diaza-bicyclo[2.2.2]octane 96%
5g
$ 2770.00

Crysdot
2,5-Diazabicyclo[2.2.2]octane 95+%
250mg
$ 454.00

Crysdot
2,5-Diazabicyclo[2.2.2]octane 95+%
1g
$ 1135.00

Chemenu
2,5-Diaza-bicyclo[2.2.2]octane 95%
1g
$ 1061.00

American Custom Chemicals Corporation
2,5-DIAZA-BICYCLO(2.2.2)OCTANE 96.00%
5MG
$ 502.24

AccelPharmtech
2,5-Diazabicyclo[2.2.2]octane 97.00%
25G
$ 9110.00

AccelPharmtech
2,5-Diazabicyclo[2.2.2]octane 97.00%
5G
$ 4850.00

AccelPharmtech
2,5-Diazabicyclo[2.2.2]octane 97.00%
1G
$ 2820.00

Total 16 raw suppliers

Chemical Property of AKOS 91597

Chemical Property:

Boiling Point:196.3±8.0 °C(Predicted)
PKA:10.76±0.20(Predicted)
PSA：24.06000
Density:0.975±0.06 g/cm3(Predicted)
LogP:0.36780

Purity/Quality:

97% ^*data from raw suppliers

2,5-Diaza-bicyclo[2.2.2]octane 96% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of AKOS 91597

There total 5 articles about AKOS 91597 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1004-98-4
2,5-diazabicyclo<2.2.2>octane-3,6-dione

: 658-24-2
2,5-diazabicyclo[2.2.2]octane

Guidance literature:: 2,5-diazabicyclo<2.2.2>octane-3,6-dione; With lithium aluminium tetrahydride; In tetrahydrofuran; for 16h; Heating / reflux;

With sodium hydroxide; water; In tetrahydrofuran; at 20 ℃; for 1h;

Reference yield:

: 54221-37-3
diethyl meso-2,5-dibromoadipate

: 658-24-2
2,5-diazabicyclo[2.2.2]octane

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium azide

2.1: hydrogenchloride; hydrogen / palladium 10% on activated carbon / ethanol; water / 20 h / 750.08 Torr

3.1: methanol; sodium methylate

4.1: lithium aluminium tetrahydride / tetrahydrofuran / 16 h / Heating / reflux

4.2: 1 h / 20 °C

With hydrogenchloride; methanol; lithium aluminium tetrahydride; sodium azide; hydrogen; sodium methylate; palladium 10% on activated carbon; In tetrahydrofuran; ethanol; water;

Reference yield:

: 54221-38-4
(2R,5S)-2,5-diazidohexanedioic acid diethyl ester

: 658-24-2
2,5-diazabicyclo[2.2.2]octane

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrogenchloride; hydrogen / palladium 10% on activated carbon / ethanol; water / 20 h / 750.08 Torr

2.1: methanol; sodium methylate

3.1: lithium aluminium tetrahydride / tetrahydrofuran / 16 h / Heating / reflux

3.2: 1 h / 20 °C

With hydrogenchloride; methanol; lithium aluminium tetrahydride; hydrogen; sodium methylate; palladium 10% on activated carbon; In tetrahydrofuran; ethanol; water;