3-Methyl-2-phenyl-2-cyclohexen-1-one

Base Information

Chemical Name:3-Methyl-2-phenyl-2-cyclohexen-1-one
CAS No.:65825-74-3
Molecular Formula:C13H14O
Molecular Weight:186.254
Hs Code.:
DSSTox Substance ID:DTXSID40459033
Nikkaji Number:J426.292A
Wikidata:Q82282632

Synonyms:3-methyl-2-phenyl-2-cyclohexen-1-one;3-methyl-2-phenylcyclohex-2-en-1-one;65825-74-3;Methylphenylcyclohexenon;2-Cyclohexen-1-one, 3-methyl-2-phenyl-;SCHEMBL22679771;DTXSID40459033

Suppliers and Price of 3-Methyl-2-phenyl-2-cyclohexen-1-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 3-Methyl-2-phenyl-2-cyclohexen-1-one

Chemical Property:

XLogP3:2.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:186.104465066
Heavy Atom Count:14
Complexity:256

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=C(C(=O)CCC1)C2=CC=CC=C2

Technology Process of 3-Methyl-2-phenyl-2-cyclohexen-1-one

There total 21 articles about 3-Methyl-2-phenyl-2-cyclohexen-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 960-16-7
tributylphenylstannane

: 140710-03-8
2-Iodo-3-methyl-2-cyclohexen-1-one

: 65825-74-3
3-methyl-2-phenylcyclohex-2-en-1-one

Guidance literature:: With copper(l) iodide; triphenyl-arsane; 1-butyl-3-methylimidazolium Tetrafluoroborate; bis(benzonitrile)palladium(II) dichloride; at 80 ℃; for 8h;
DOI:10.1021/ol0068849

Reference yield: 88.0%

: 1352617-28-7
3-methyl-2-phenylcyclohex-1-enyl t-butyldimethylsilyl ether

: 65825-74-3
3-methyl-2-phenylcyclohex-2-en-1-one

Guidance literature:: 3-methyl-2-phenylcyclohex-1-enyl t-butyldimethylsilyl ether; With (x)BF₄*C₉H₁₄NO⁽¹⁺⁾; In dichloromethane; at -78 ℃; for 1h;

With sodium hydrogencarbonate; In dichloromethane; water; at 20 ℃;
DOI:10.1021/ol2029417

Reference yield: 78.0%

: 140710-03-8
2-Iodo-3-methyl-2-cyclohexen-1-one

: 98-80-6
phenylboronic acid

: 65825-74-3
3-methyl-2-phenylcyclohex-2-en-1-one

Guidance literature:: With sodium carbonate; palladium on activated charcoal; In 1,2-dimethoxyethane; water; at 50 ℃; for 12h;
DOI:10.1021/jo051501b