Ethanone, 1-(5-methyl-2-benzothiazolyl)- (9CI)

Base Information

Chemical Name:Ethanone, 1-(5-methyl-2-benzothiazolyl)- (9CI)
CAS No.:65840-55-3
Molecular Formula:C10H9NOS
Molecular Weight:191.25000
Hs Code.:2934999090

Synonyms:5-methyl-2-acetyl-1,2,3-diazaphosphole;2-Acetyl-5-methylbenzothiazol;2H-1,2,3-Diazaphosphole,2-acetyl-5-methyl;2-phenyl-5-methyl-1,2,3-diazaphosphole;2-acetyl-5-methyldiazaphosphole;2-Acetyl-5-methyl-1,2,3-diazaphosphole;4-Methyl-2-acetyl-1,2,3-phosphadiazol;2-acetyl-5-methyl-2H-1,2,3-diazaphosphole;

Suppliers and Price of Ethanone, 1-(5-methyl-2-benzothiazolyl)- (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
1-(5-METHYLBENZO[D]THIAZOL-2-YL)ETHANONE 95.00%
5MG
$ 501.05

Total 1 raw suppliers

Chemical Property of Ethanone, 1-(5-methyl-2-benzothiazolyl)- (9CI)

Chemical Property:

PSA：58.20000
LogP:2.80730

Purity/Quality:: 1-(5-METHYLBENZO[D]THIAZOL-2-YL)ETHANONE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Ethanone, 1-(5-methyl-2-benzothiazolyl)- (9CI)

There total 4 articles about Ethanone, 1-(5-methyl-2-benzothiazolyl)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: C₁₂H₁₃NO₂S

: 65840-55-3
1-(5-methylbenzo[d]thiazol-2-yl)ethan-1-one

Guidance literature:: With hydrogenchloride; In water; acetone; at 20 ℃; for 8h;
DOI:10.1039/d1cc00621e

Reference yield:

: 14779-17-0
2-amino-5-methylbenzothiazole

: 65840-55-3
1-(5-methylbenzo[d]thiazol-2-yl)ethan-1-one

Guidance literature:: Multi-step reaction with 3 steps

1: isopentyl nitrite / tetrahydrofuran / 0.5 h / Schlenk technique; Reflux

2: tert.-butylhydroperoxide; iron(II) triflate / decane; 1,2-dichloro-ethane / 48 h / 35 °C

3: hydrogenchloride / acetone; water / 8 h / 20 °C

With iron(II) triflate; hydrogenchloride; tert.-butylhydroperoxide; isopentyl nitrite; In tetrahydrofuran; decane; water; 1,2-dichloro-ethane; acetone;
DOI:10.1039/d1cc00621e

Reference yield:

: 2942-16-7
5-methylbenzo[d]thiazole

: 65840-55-3
1-(5-methylbenzo[d]thiazol-2-yl)ethan-1-one

Guidance literature:: Multi-step reaction with 2 steps

1: tert.-butylhydroperoxide; iron(II) triflate / decane; 1,2-dichloro-ethane / 48 h / 35 °C

2: hydrogenchloride / acetone; water / 8 h / 20 °C

With iron(II) triflate; hydrogenchloride; tert.-butylhydroperoxide; In decane; water; 1,2-dichloro-ethane; acetone;
DOI:10.1039/d1cc00621e