2-Amino-2'-chloro-5-nitrobenzophenone

Base Information

Chemical Name:2-Amino-2'-chloro-5-nitrobenzophenone
CAS No.:2011-66-7
Molecular Formula:C13H9ClN2O3
Molecular Weight:276.679
Hs Code.:29223990
European Community (EC) Number:217-929-4
UNII:RL4AJ2Z1GR
DSSTox Substance ID:DTXSID20173927
Nikkaji Number:J133.148E
Wikidata:Q72434577
Mol file:2011-66-7.mol

Synonyms:2-amino-2'-chloro-5-nitrobenzophenone

Suppliers and Price of 2-Amino-2'-chloro-5-nitrobenzophenone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

AHH
2-Amino-2-chloro-5-nitrobenzophenone 98%
100g
$ 380.00

AK Scientific
Clonazepam Related Compound B
100mg
$ 80.00

Alfa Aesar
2-Amino-2'-chloro-5-nitrobenzophenone, 98%
25g
$ 96.20

Alfa Aesar
2-Amino-2'-chloro-5-nitrobenzophenone, 98%
5g
$ 26.60

Alfa Aesar
2-Amino-2'-chloro-5-nitrobenzophenone, 98%
100g
$ 306.00

Alichem
(2-Amino-5-nitrophenyl)(2-chlorophenyl)methanone
500g
$ 408.10

Ambeed
(2-Amino-5-nitrophenyl)(2-chlorophenyl)methanone 97%
25g
$ 37.00

Ambeed
(2-Amino-5-nitrophenyl)(2-chlorophenyl)methanone 97%
5g
$ 11.00

Ambeed
(2-Amino-5-nitrophenyl)(2-chlorophenyl)methanone 97%
10g
$ 20.00

Ambeed
(2-Amino-5-nitrophenyl)(2-chlorophenyl)methanone 97%
100g
$ 118.00

Total 98 raw suppliers

Chemical Property of 2-Amino-2'-chloro-5-nitrobenzophenone

Chemical Property:

Appearance/Colour:yellow crystal powder
Melting Point:157-163oC
Boiling Point:505.8 °C at 760 mmHg
PKA:-3.12±0.36(Predicted)
Flash Point:259.7 °C
PSA：88.91000
Density:1.428 g/cm³
LogP:4.16580
Storage Temp.:Refrigerator, Under Inert Atmosphere
Sensitive.:Air Sensitive
Solubility.:Chloroform (Slightly), Methanol (Slightly)
XLogP3:3.6
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:2
Exact Mass:276.0301698
Heavy Atom Count:19
Complexity:358

Purity/Quality:

98% ^*data from raw suppliers

2-Amino-2-chloro-5-nitrobenzophenone 98% ^*data from reagent suppliers

Safty Information:

Pictogram(s): Xi
Hazard Codes:Xi
Statements: 46-36/37/38
Safety Statements: 53-26-36/37-60

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C(=C1)C(=O)C2=C(C=CC(=C2)[N+](=O)[O-])N)Cl
Uses 2-Amino-5-nitro-2''-chlorobenzophenone (Clonazepam EP Impurity A) is an impurity of Clonazepam (C587080).

Technology Process of 2-Amino-2'-chloro-5-nitrobenzophenone

There total 10 articles about 2-Amino-2'-chloro-5-nitrobenzophenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 17420-30-3
5-nitroanthranilonitrile

: 3900-89-8
2-Chlorobenzeneboronic acid

: 2011-66-7
2'-chloro-5-nitro-2-aminobenzophenone

Guidance literature:: With 5,5'-dimethyl-2,2'-bipyridine; methanesulfonic acid; palladium(II) trifluoroacetate; water; In 2-methyltetrahydrofuran; at 100 ℃; for 36h; Reagent/catalyst; Solvent; Sealed tube; Inert atmosphere; Cooling with ice;

Reference yield: 94.0%

: potassium (2-amino-5-nitrophenyl)trifluoroboranuide

: 609-65-4
o-chlorobenzoyl chloride

: 2011-66-7
2'-chloro-5-nitro-2-aminobenzophenone

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In water; toluene; at 90 ℃; for 12h; Reagent/catalyst; Temperature; Solvent;