2-chloromethyl-4-o-chlorophenyl-1,2-dihydro-6-nitro-quinazoline 3-oxide

Base Information

Chemical Name:2-chloromethyl-4-o-chlorophenyl-1,2-dihydro-6-nitro-quinazoline 3-oxide
CAS No.:101945-55-5
Molecular Formula:C₁₅H₁₁Cl₂N₃O₃
Molecular Weight:352.177
Hs Code.:

Synonyms:2-chloromethyl-4-o-chlorophenyl-1,2-dihydro-6-nitro-quinazoline 3-oxide

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Chemical Property of 2-chloromethyl-4-o-chlorophenyl-1,2-dihydro-6-nitro-quinazoline 3-oxide

Chemical Property:

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Technology Process of 2-chloromethyl-4-o-chlorophenyl-1,2-dihydro-6-nitro-quinazoline 3-oxide

There total 1 articles about 2-chloromethyl-4-o-chlorophenyl-1,2-dihydro-6-nitro-quinazoline 3-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 97-97-2
chloroacetaldehyde dimethyl acetal

: 2011-66-7
2'-chloro-5-nitro-2-aminobenzophenone

: 101945-55-5
2-chloromethyl-4-o-chlorophenyl-1,2-dihydro-6-nitro-quinazoline 3-oxide

Guidance literature:: With hydrogenchloride; hydroxylamine; In ethanol; water; 1.) 2 h; 2.) 2.5 h, reflux;

Reference yield: 75.0%

: 101945-55-5
2-chloromethyl-4-o-chlorophenyl-1,2-dihydro-6-nitro-quinazoline 3-oxide

: 101928-09-0
2-chloromethyl-4-o-chlorophenyl-6-nitro-quinazoline 3-oxide

Guidance literature:: With manganese(IV) oxide; In dichloromethane; for 20h; Ambient temperature;

Reference yield:

: 101945-55-5
2-chloromethyl-4-o-chlorophenyl-1,2-dihydro-6-nitro-quinazoline 3-oxide

: 101928-18-1
6-o-chlorophenyl-2,4-dihydro-2(4-methyl-1-piperazinyl)methylene-8-nitro-1H-imidazo<1,2-a><1,4>benzodiazepin-1-one 5-oxide

Guidance literature:: Multi-step reaction with 6 steps

1: 75 percent / MnO₂ / CH₂Cl₂ / 20 h / Ambient temperature

2: 80 percent / methanol / 2 h / Ambient temperature

3: 90 percent / imidazole / 48 h / Heating

4: 55 percent / 2 N NaOH / dimethylformamide / 5 °C

5: 1.) dicyclohexylcarbodiimide; 2.) triethylamine / 1.) CH₂Cl₂, 1 h, RT; 2.) 2 h

6: 70 percent / toluene / 9 h / Heating

With 1H-imidazole; manganese(IV) oxide; sodium hydroxide; triethylamine; dicyclohexyl-carbodiimide; In methanol; dichloromethane; N,N-dimethyl-formamide; toluene;