Benzoic acid, 4-iodo-, sodiuM salt

Base Information

• Chemical Name: Benzoic acid, 4-iodo-, sodiuM salt
• CAS No.: 1005-30-7
• Molecular Formula: C7H5 I O2 . Na
• Molecular Weight: 270.002
• Hs Code.: 2916399090
• Mol file: 1005-30-7.mol

Synonyms:Benzoicacid, 4-iodo-, sodium salt (9CI); Benzoic acid, p-iodo-, sodium salt (8CI);Sodium 4-iodobenzoate; Sodium p-iodobenzoate

Chemical Property of Benzoic acid, 4-iodo-, sodiuM salt

Chemical Property:

• Vapor Pressure: 0.00015mmHg at 25°C
• Boiling Point: 318.5°Cat760mmHg
• Flash Point: 146.4°C
• PSA: 40.13000
• Density: g/cm³
• LogP: 0.65470

Purity/Quality:

98%,99%, ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Benzoic acid, 4-iodo-, sodiuM salt

There total 3 articles about Benzoic acid, 4-iodo-, sodiuM salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

4-iodobenzoic acid (619-58-9) → sodium 4-iodo-benzoate (1005-30-7)

Guidance literature:

With sodium hydroxide; In water; at 70 ℃;

DOI:10.1142/S1088424610002641

Reference yield:

4-iodobenzoic acid (619-58-9) + 4-nitrophenol sodium salt (824-78-2) → 4-nitro-phenol (100-02-7,78813-13-5,89830-32-0) + sodium 4-iodo-benzoate (1005-30-7)

Guidance literature:

With 1-butyl-2,3-dimethylimidazolium bis-(trifluoromethanesulfonyl)amide; In methanol; at 24.84 ℃; Reagent/catalyst; Equilibrium constant;

DOI:10.1021/jo100914p

Reference yield:

sodium methylate (124-41-4) + Acetic acid 2-(4-iodo-phenyl)-2-oxo-1-phenyl-ethyl ester (119267-73-1) → Dimethyl ether (115-10-6,157621-61-9) + Benzyl acetate (140-11-4) + sodium 4-iodo-benzoate (1005-30-7)

Guidance literature:

In methanol; at 20 ℃; Rate constant;

upstream raw materials:

sodium methylate

Acetic acid 2-(4-iodo-phenyl)-2-oxo-1-phenyl-ethyl ester

4-iodobenzoic acid

4-nitrophenol sodium salt

Downstream raw materials:

<2-(4-Jod-benzoyloxy)-propionsaeure>-propylester

4-Propionoxybutyl p-Iodobenzoate

<4-(4-Jod-benzoyloxy)-buttersaeure>-butylester

<4-(4-Jod-benzoyloxy)-buttersaeure>-<3-methyl-butylester>

Refernces

• 1、 D'Anna, Francesca,Marullo, Salvatore,Vitale, Paola,Noto, Renato. "Electronic and steric effects: How do they work in ionic liquids? the case of benzoic acid dissociation". experimental part. p. 4828 - 4834. Retrieved 2010/10/04.
• 2、 Morozov, A. A.. "CLEAVAGE OF THE PHENACYL ESTERS OF CARBOXYLIC AND THIOCARBOXYLIC ACIDS BY METAL ALKOXIDES". . p. 1138 - 1143. Retrieved 2007/10/02.