n-(2,6-Dimethyl-4-nitrophenyl)-4-methylbenzenesulfonamide

Base Information

Chemical Name:n-(2,6-Dimethyl-4-nitrophenyl)-4-methylbenzenesulfonamide
CAS No.:67083-22-1
Molecular Formula:C15H16N2O4S
Molecular Weight:320.369
Hs Code.:
NSC Number:101581,97147
DSSTox Substance ID:DTXSID50294573
Wikidata:Q82033945
ChEMBL ID:CHEMBL1704200

Synonyms:MLS002703379;67083-22-1;n-(2,6-dimethyl-4-nitrophenyl)-4-methylbenzenesulfonamide;NSC97147;CHEMBL1704200;SCHEMBL10623079;DTXSID50294573;FMQFWJMJTOKIET-UHFFFAOYSA-N;NSC-97147;NSC101581;NSC-101581;SMR001570098;1-(p-Toluenesulfonamido)-2,6-dimethyl-4-nitrobenzene

Suppliers and Price of n-(2,6-Dimethyl-4-nitrophenyl)-4-methylbenzenesulfonamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of n-(2,6-Dimethyl-4-nitrophenyl)-4-methylbenzenesulfonamide

Chemical Property:

Vapor Pressure:1.36E-09mmHg at 25°C
Boiling Point:485.9°Cat760mmHg
Flash Point:247.6°C
Density:1.339g/cm³
XLogP3:3.4
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:3
Exact Mass:320.08307817
Heavy Atom Count:22
Complexity:477

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=C(C=C1)S(=O)(=O)NC2=C(C=C(C=C2C)[N+](=O)[O-])C

Technology Process of n-(2,6-Dimethyl-4-nitrophenyl)-4-methylbenzenesulfonamide

There total 5 articles about n-(2,6-Dimethyl-4-nitrophenyl)-4-methylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 4703-15-5
N-(2,6-dimethylphenyl)-4-methylbenzenesulfonamide

: 67083-22-1
N-(2,6-dimethyl-4-nitrophenyl)-4-methylbenzenesulfonamide

Guidance literature:: With sodium nitrate; nitric acid; acetic acid; In water; at 0 ℃; for 4h; Reflux;

Reference yield:

: 87-62-7
2,6-dimethylaniline

: 67083-22-1
N-(2,6-dimethyl-4-nitrophenyl)-4-methylbenzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: 61 percent / pyridine / 4 h / Heating

2: 74 percent / conc. HNO₃ / acetic acid; H₂O / 4 h / 140 °C

With pyridine; nitric acid; In water; acetic acid;
DOI:10.1039/b617576g

Reference yield:

: 98-59-9
p-toluenesulfonyl chloride

: 67083-22-1
N-(2,6-dimethyl-4-nitrophenyl)-4-methylbenzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / 16 h

2: sodium nitrite; nitric acid / acetic acid; water / 3 h / 140 °C

With nitric acid; sodium nitrite; In pyridine; water; acetic acid;
DOI:10.1021/acs.macromol.6b00351