5-Hexenal, 4-(dimethylphenylsilyl)-

Base Information

Chemical Name:5-Hexenal, 4-(dimethylphenylsilyl)-
CAS No.:663176-43-0
Molecular Formula:C14H20OSi
Molecular Weight:232.398
Hs Code.:

Synonyms:

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Chemical Property of 5-Hexenal, 4-(dimethylphenylsilyl)-

Chemical Property:

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Technology Process of 5-Hexenal, 4-(dimethylphenylsilyl)-

There total 4 articles about 5-Hexenal, 4-(dimethylphenylsilyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6-(dimethyl-phenyl-silanyl)-1-phenyl-oct-7-ene-2,3-diol

: 663176-43-0
4-(dimethyl-phenyl-silanyl)-hex-5-enal

Guidance literature:: With sodium periodate; In tetrahydrofuran; methanol; water; at 20 ℃; for 1.5h;
DOI:10.1021/ol061914e

Reference yield:

: 768-33-2
phenyldimethylsilyl chloride

: 663176-43-0
4-(dimethyl-phenyl-silanyl)-hex-5-enal

Guidance literature:: Multi-step reaction with 3 steps

1: Ni(acac)2 / tetrahydrofuran / 20 h / -20 °C

2: K₃Fe(CN)6; K₂CO₃; potassium osmium dihydrate / (DHQD)2PYR; methanesulfonamide / 2-methyl-propan-2-ol; H₂O / 30 h / 20 °C

3: 6.60 g / sodium periodate / methanol; tetrahydrofuran; H₂O / 1.5 h / 20 °C

With bis(acetylacetonate)nickel(II); sodium periodate; potassium osmium dihydrate; potassium carbonate; potassium hexacyanoferrate(III); hydroquinindine-2,5-diphenyl-4,6-pyrimidinediyl diether; methanesulfonamide; In tetrahydrofuran; methanol; water; tert-butyl alcohol;
DOI:10.1021/ol061914e

Reference yield:

: 607732-69-4
Dimethyl-phenyl-((E)-6-phenyl-1-vinyl-hex-4-enyl)-silane

: 663176-43-0
4-(dimethyl-phenyl-silanyl)-hex-5-enal

Guidance literature:: Multi-step reaction with 2 steps

1: K₃Fe(CN)6; K₂CO₃; potassium osmium dihydrate / (DHQD)2PYR; methanesulfonamide / 2-methyl-propan-2-ol; H₂O / 30 h / 20 °C

2: 6.60 g / sodium periodate / methanol; tetrahydrofuran; H₂O / 1.5 h / 20 °C

With sodium periodate; potassium osmium dihydrate; potassium carbonate; potassium hexacyanoferrate(III); hydroquinindine-2,5-diphenyl-4,6-pyrimidinediyl diether; methanesulfonamide; In tetrahydrofuran; methanol; water; tert-butyl alcohol;
DOI:10.1021/ol061914e