Benzenemethanamine, N-[(4-nitrophenyl)methylene]-a-phenyl-

Base Information

Chemical Name:Benzenemethanamine, N-[(4-nitrophenyl)methylene]-a-phenyl-
CAS No.:66607-69-0
Molecular Formula:C20H16N2O2
Molecular Weight:316.359
Hs Code.:

Synonyms:Benzhydryl-(4-nitro-benzyliden)-amin;benzhydryl-(4-nitro-benzyliden)-amine;N-(diphenylmethyl)-p-nitrophenylmethanimine;4-Nitro-benzaldehyd-benzhydrylimin;

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzenemethanamine, N-[(4-nitrophenyl)methylene]-a-phenyl-

Chemical Property:

Melting Point:134-135 °C
Boiling Point:466.1±45.0 °C(Predicted)
PSA：58.18000
Density:1.13±0.1 g/cm3(Predicted)
LogP:5.32650

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Benzenemethanamine, N-[(4-nitrophenyl)methylene]-a-phenyl-

There total 1 articles about Benzenemethanamine, N-[(4-nitrophenyl)methylene]-a-phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 555-16-8
4-nitrobenzaldehdye

: 91-00-9
Benzhydrylamine

: 66607-69-0
4-nitrobenzylidenediphenylmethylamine

Guidance literature:: With zinc(II) chloride; In toluene; for 0.5h; Heating;

Reference yield: 97.0%

: 66607-69-0
N-(4-nitrobenzylidene)-1,1-diphenylmethanimine

: 4559-70-0
Diphenylphosphine oxide

: 1282607-17-3
(-)-N-benzhydryl(diphenylphosphoryl)(4-nitrophenyl)methanamine

Guidance literature:: With 2C₄₈H₂₈O₄P^(1-)*Mg⁽²⁺⁾; In acetonitrile; at 20 ℃; for 12h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1021/ol200456y

Reference yield: 96.0%

: 623-73-4
diazoacetic acid ethyl ester

: 66607-69-0
N-(4-nitrobenzylidene)-1,1-diphenylmethanimine

: cis-1-benzhydryl-(2R)-(4-nitrophenyl)-aziridine-(2R)-carboxylic scid ethyl ester

Guidance literature:: N-(4-nitrobenzylidene)-1,1-diphenylmethanimine; With triphenylborane; 7,7’-di-t-butyl VANOL; water; In toluene; at 20 ℃; for 0.0833333h;

diazoacetic acid ethyl ester; In toluene; at 20 ℃; for 24h;
DOI:10.1002/chem.201302451