Benzenesulfonic acid, 4-(2,3,6,7-tetrahydro-2,6-dioxo-1-propyl-1H-purin-8-yl)-, 3-nitrophenyl ester

Base Information

Chemical Name:Benzenesulfonic acid, 4-(2,3,6,7-tetrahydro-2,6-dioxo-1-propyl-1H-purin-8-yl)-, 3-nitrophenyl ester
CAS No.:666716-03-6
Molecular Formula:C20H17N5O7S
Molecular Weight:471.45
Hs Code.:

Synonyms:

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Chemical Property of Benzenesulfonic acid, 4-(2,3,6,7-tetrahydro-2,6-dioxo-1-propyl-1H-purin-8-yl)-, 3-nitrophenyl ester

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Technology Process of Benzenesulfonic acid, 4-(2,3,6,7-tetrahydro-2,6-dioxo-1-propyl-1H-purin-8-yl)-, 3-nitrophenyl ester

There total 6 articles about Benzenesulfonic acid, 4-(2,3,6,7-tetrahydro-2,6-dioxo-1-propyl-1H-purin-8-yl)-, 3-nitrophenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 666715-95-3
6-amino-3-propyl-5-[4-[[m-nitrophenoxy]sulfonyl]benzamido]uracil

: 666716-03-6
4-(2,6-dioxo-1-propyl-2,3,6,7-tetrahydro-1H-purin-8-yl)-benzenesulfonic acid 3-nitro-phenyl ester

Guidance literature:: With polyphosphoric acid trimethylsilyl ester; at 120 - 170 ℃;
DOI:10.1021/jm0310030

Reference yield:

: 554-84-7
meta-nitrophenol

: 666716-03-6
4-(2,6-dioxo-1-propyl-2,3,6,7-tetrahydro-1H-purin-8-yl)-benzenesulfonic acid 3-nitro-phenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: Tris-HCl buffer; aq. NaOH / tetrahydrofuran / 4 h / 20 °C / pH 8 - 9

2: N-(3-(dimethylamino)propyl)-N-ethylcarbodiimide*HCl / methanol / 20 °C

3: polyphosphoric acid trimethylsilyl ester / 120 - 170 °C

With sodium hydroxide; polyphosphoric acid trimethylsilyl ester; Tris-HCl buffer; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; methanol;
DOI:10.1021/jm0310030

Reference yield:

: 10130-89-9
p-carboxyphenylsulfonyl chloride

: 666716-03-6
4-(2,6-dioxo-1-propyl-2,3,6,7-tetrahydro-1H-purin-8-yl)-benzenesulfonic acid 3-nitro-phenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: Tris-HCl buffer; aq. NaOH / tetrahydrofuran / 4 h / 20 °C / pH 8 - 9

2: N-(3-(dimethylamino)propyl)-N-ethylcarbodiimide*HCl / methanol / 20 °C

3: polyphosphoric acid trimethylsilyl ester / 120 - 170 °C

With sodium hydroxide; polyphosphoric acid trimethylsilyl ester; Tris-HCl buffer; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; methanol;
DOI:10.1021/jm0310030