S-(2,6-Dimethylphenyl) 2,6-dimethylbenzene-1-sulfinothioate

Base Information

Chemical Name:S-(2,6-Dimethylphenyl) 2,6-dimethylbenzene-1-sulfinothioate
CAS No.:66713-32-4
Molecular Formula:C16H18OS2
Molecular Weight:290.45
Hs Code.:
DSSTox Substance ID:DTXSID10495842

Synonyms:66713-32-4;DTXSID10495842;S-(2,6-Dimethylphenyl) 2,6-dimethylbenzene-1-sulfinothioate

Suppliers and Price of S-(2,6-Dimethylphenyl) 2,6-dimethylbenzene-1-sulfinothioate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of S-(2,6-Dimethylphenyl) 2,6-dimethylbenzene-1-sulfinothioate

Chemical Property:

XLogP3:4.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:290.07990754
Heavy Atom Count:19
Complexity:298

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C(C(=CC=C1)C)SS(=O)C2=C(C=CC=C2C)C

Technology Process of S-(2,6-Dimethylphenyl) 2,6-dimethylbenzene-1-sulfinothioate

There total 6 articles about S-(2,6-Dimethylphenyl) 2,6-dimethylbenzene-1-sulfinothioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 15.0%

: 66713-28-8
tert-Butyl 2,6-xylyl sulfoxide

: 2905-17-1
bis(2,6-dimethylphenyl)disulfide

: 66713-32-4
2,6-Xylyl 2,6-xylenethiosulfinate

: 66713-33-5
2,6-Xylyl 2,5-xylenethiosulfonate

Guidance literature:: With propynoic acid methyl ester; In toluene; at 520 ℃; flash vacuum pyrolysis;
DOI:10.1021/jo00330a017

Reference yield:

: 66713-28-8
tert-Butyl 2,6-xylyl sulfoxide

: 66713-32-4
2,6-Xylyl 2,6-xylenethiosulfinate

Guidance literature:: With propynoic acid methyl ester; In toluene; at 520 ℃;
DOI:10.1016/S0040-4039(01)85053-X

Reference yield:

: 2905-17-1
bis(2,6-dimethylphenyl)disulfide

: 66713-32-4
2,6-Xylyl 2,6-xylenethiosulfinate

Guidance literature:: Multi-step reaction with 3 steps

1: pentane / 2 h / Ambient temperature

2: 90 percent / m-chloroperbenzoic acid / CHCl₃ / 1.) 0 deg C, 2.) 0.5 h, room temp.

3: 65 percent / methyl propiolate / toluene / 520 °C / flash vacuum pyrolysis

With propynoic acid methyl ester; 3-chloro-benzenecarboperoxoic acid; In chloroform; toluene; pentane;
DOI:10.1021/jo00330a017