Technology Process of Bromotris(2,5-dimethylphenyl)stannane
There total 2 articles about Bromotris(2,5-dimethylphenyl)stannane which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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In
diethyl ether; toluene;
addn. of soln. of SnBr4 in toluene to ether soln. of grignard-reagent (prepd. from Mg and org. compd.), heating (6 h), cooling; hydrolization (H2O and aq. HBr), washing of org. layer (H2O, dild. soln. of NaHCO3 and H2O), drying (Na2SO4), removal of solvent;
- Guidance literature:
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/1503350200032/;
- Guidance literature:
-
In
diethyl ether; toluene;
addn. of soln. of SnBr4 in toluene to ether soln. of grignard-reagent (prepd. from Mg and org. compd.), removal of ether, heating (boiling point of toluene, 2 h), cooling; hydrolization (dild. HBr), sepn. of org. layer, washing, drying (Na2SO4), removal of solvent, recrystn. (propyl or butyl alcohol); elem. anal.;