Sn{2,5-dimethyl-phenyl}4

Base Information

Chemical Name:Sn{2,5-dimethyl-phenyl}4
CAS No.:6746-23-2
Molecular Formula:C₃₂H₃₆Sn
Molecular Weight:539.348
Hs Code.:

Synonyms:Sn{2,5-dimethyl-phenyl}4

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Chemical Property of Sn{2,5-dimethyl-phenyl}4

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Technology Process of Sn{2,5-dimethyl-phenyl}4

There total 3 articles about Sn{2,5-dimethyl-phenyl}4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 7646-78-8
tin(IV) chloride

: 30897-86-0
2,5-dimethylphenylmagnesium bromide

: 6746-23-2
Sn{2,5-dimethyl-phenyl}4

Guidance literature:: In tetrahydrofuran; addn. of a soln. of SnCl4 to a soln. of organic compound under cooling, heating for 12 h under reflux; addn. of HCl, reccrystn., elem. anal.;
DOI:10.1016/0022-328X(94)80074-X

Reference yield: 35.0%

: 553-94-6
4-bromo-m-xylene

: 7439-95-4
magnesium

: 6674-67-5
{2,5-(CH₃)2C₆H₃}3SnBr

: 6746-23-2
Sn{2,5-dimethyl-phenyl}4

Guidance literature:: In diethyl ether; toluene; addn. of soln. of SnBr4 in toluene to ether soln. of grignard-reagent (prepd. from Mg and org. compd.), removal of ether, heating (boiling point of toluene, 15 h), cooling; hydrolization (dild. HBr), sepn. of org. layer, washing, drying (Na2SO4), removal of solvent, recrystn. (propyl or butyl alcohol); elem. anal.;