N-allyl-2-chlorobenzamide

Base Information

Chemical Name:N-allyl-2-chlorobenzamide
CAS No.:66896-68-2
Molecular Formula:C10H10ClNO
Molecular Weight:195.648
Hs Code.:
DSSTox Substance ID:DTXSID30390547
Nikkaji Number:J1.835.119F
Wikidata:Q82187391
ChEMBL ID:CHEMBL1372645

Synonyms:N-allyl-2-chlorobenzamide;66896-68-2;N-allyl-2-chlorobenzenecarboxamide;N-Allyl-2-chloro-benzamide;2-chloro-N-prop-2-enylbenzamide;SMR000023909;MLS000087688;Benzamide, 2-chloro-N-allyl-;CHEMBL1372645;DTXSID30390547;RRTKKTTXRXQMEF-UHFFFAOYSA-N;HMS2433C08;MFCD00794699;AKOS001604647;2-chloro-N-(prop-2-en-1-yl)benzamide;7L-922;SR-01000414913;SR-01000414913-1

Suppliers and Price of N-allyl-2-chlorobenzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of N-allyl-2-chlorobenzamide

Chemical Property:

XLogP3:1.5
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:3
Exact Mass:195.0450916
Heavy Atom Count:13
Complexity:193

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C=CCNC(=O)C1=CC=CC=C1Cl

Technology Process of N-allyl-2-chlorobenzamide

There total 3 articles about N-allyl-2-chlorobenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 609-65-4
o-chlorobenzoyl chloride

: 107-11-9,30551-89-4
1-amino-2-propene

: 66896-68-2
N-allyl-2-chloro-benzamide

Guidance literature:: With pyridine; In tetrahydrofuran; at 20 ℃; for 0.75h;
DOI:10.1021/jo026763h

Reference yield: 80.0%

: 107-11-9,30551-89-4
1-amino-2-propene

: 118-91-2
ortho-chlorobenzoic acid

: 66896-68-2
N-allyl-2-chloro-benzamide

Guidance literature:: With 1-ethyl-3-(3-dimethyl-aminopropyl) carbodiimide; benzotriazol-1-ol; triethylamine; In dichloromethane; at 20 ℃;
DOI:10.1021/acs.orglett.8b03682

Reference yield: 77.0%

: 694-80-4
2-bromo-1-chlorobenzene

: 201230-82-2
carbon monoxide

: 107-11-9,30551-89-4
1-amino-2-propene

: 66896-68-2
N-allyl-2-chloro-benzamide

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; 1,8-diazabicyclo[5.4.0]undec-7-ene; at 110 ℃; for 24h; under 760.051 Torr; Ionic liquid; Autoclave;
DOI:10.1021/ol101714p