6-Methoxy-1,2-dihydrobenzocyclobutene-1-ol

Base Information

Chemical Name:6-Methoxy-1,2-dihydrobenzocyclobutene-1-ol
CAS No.:66947-61-3
Molecular Formula:C9H10O2
Molecular Weight:150.177
Hs Code.:
DSSTox Substance ID:DTXSID001241295
Nikkaji Number:J623.185C

Synonyms:6-Methoxybenzocyclobutan-1-ol;SCHEMBL7542801;SWKMXWZMFAAWGA-UHFFFAOYSA-N;DTXSID001241295;66947-61-3;6-Methoxy-1,2-dihydrobenzocyclobutene-1-ol;Bicyclo[4.2.0]octa-1,3,5-trien-7-ol, 5-methoxy-

Suppliers and Price of 6-Methoxy-1,2-dihydrobenzocyclobutene-1-ol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 6-Methoxy-1,2-dihydrobenzocyclobutene-1-ol

Chemical Property:

XLogP3:0.3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:150.068079557
Heavy Atom Count:11
Complexity:147

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:COC1=CC=CC2=C1C(C2)O

Technology Process of 6-Methoxy-1,2-dihydrobenzocyclobutene-1-ol

There total 2 articles about 6-Methoxy-1,2-dihydrobenzocyclobutene-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 412304-80-4
methyl 5-phenylpenta-2,4-diynoate

: 54884-55-8
2-methoxy-6-methyl-benzaldehyde

: 66947-61-3
5-methoxybicyclo[4.2.0]octa-1,3,5-trien-7-ol

: methyl 5-methoxy-3-(phenylethynyl)-2-naphthoate

Guidance literature:: In toluene; at 20 ℃; for 0.5h; regioselective reaction; Irradiation; Sealed tube; Inert atmosphere;
DOI:10.1021/jacs.0c02002

Reference yield:

: 2944-49-2
2,3-dimethylanisole

: 66947-61-3
5-methoxybicyclo[4.2.0]octa-1,3,5-trien-7-ol

: methyl 5-methoxy-3-(phenylethynyl)-2-naphthoate

Guidance literature:: Multi-step reaction with 2 steps

1: copper(ll) sulfate pentahydrate; dipotassium peroxodisulfate / acetonitrile; water / 1 h / 90 °C

2: toluene / 0.5 h / 20 °C / Irradiation; Sealed tube; Inert atmosphere

With dipotassium peroxodisulfate; copper(ll) sulfate pentahydrate; In water; toluene; acetonitrile;
DOI:10.1021/jacs.0c02002