N,N''-Ethylenebis[N-methyl-p-phenylenediamine]

Base Information

• Chemical Name: N,N''-Ethylenebis[N-methyl-p-phenylenediamine]
• CAS No.: 29103-75-1
• Molecular Formula: C16H22 N4
• Molecular Weight: 270.377
• Hs Code.: 2921590090
• Mol file: 29103-75-1.mol

Synonyms:1,4-Benzenediamine,N,N''-1,2-ethanediylbis[N-methyl- (9CI); p-Phenylenediamine,N,N''-ethylenebis[N-methyl- (8CI); 2,5-Bis(4-aminophenyl)-2,5-diazahexane;N,N'-Bis(4-aminophenyl)-N,N'-dimethylethylenediamine;N,N''-Ethylenebis[N-methyl-p-phenylenediamine]; NSC 129674

Chemical Property of N,N''-Ethylenebis[N-methyl-p-phenylenediamine]

Chemical Property:

• Boiling Point: 476.4°Cat760mmHg
• PKA: 7.40±0.50(Predicted)
• Flash Point: 275.7°C
• PSA: 58.52000
• Density: 1.171g/cm³
• LogP: 3.58600
• Storage Temp.: Keep in dark place,Inert atmosphere,Room temperature

Purity/Quality:

99.9% ^*data from raw suppliers

N1,N1'-(Ethane-1,2-diyl)bis(N1-methylbenzene-1,4-diamine) 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N,N''-Ethylenebis[N-methyl-p-phenylenediamine]

There total 1 articles about N,N''-Ethylenebis[N-methyl-p-phenylenediamine] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

N,N'-bis(4-nitrophenyl)-N,N'-dimethylethane-1,2-diamine → N,N'-bis(4-aminophenyl)-N,N'-dimethylethane-1,2-diamine (29103-75-1)

Guidance literature:

With 5%-palladium/activated carbon; hydrogen; In methanol; at 50 ℃; for 72h;

Reference yield: 88.0%

N,N'-bis(4-aminophenyl)-N,N'-dimethylethane-1,2-diamine (29103-75-1) + acetone (67-64-1) → N,N'-bis[4-(isopropylamino)phenyl]-N,N'-dimethylethane-1,2-diamine

Guidance literature:

N,N'-bis(4-aminophenyl)-N,N'-dimethylethane-1,2-diamine; acetone; With sodium cyanoborohydride; acetic acid; In methanol; at 20 ℃; for 3h; pH=6.5 - 7.5; Cooling with ice;

With sodium hydroxide; In water; at 20 ℃; for 1h;

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