Chloro(chloromethyl)dimethylgermane

Base Information

Chemical Name:Chloro(chloromethyl)dimethylgermane
CAS No.:6727-64-6
Molecular Formula:C₃H₈Cl₂Ge
Molecular Weight:187.593
Hs Code.:2931900090
Mol file:6727-64-6.mol

Synonyms:Chlormethyldimethylchlorgerman;Chlormethyl-dimethyl-chlorgerman;Chlor-chlormethyl-dimethyl-german;Chlor(chlormethyl)dimethylgerman;Chlor-dimethyl-chlormethyl-german;

Suppliers and Price of Chloro(chloromethyl)dimethylgermane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of Chloro(chloromethyl)dimethylgermane

Chemical Property:

PSA：0.00000
LogP:2.62660

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Chloro(chloromethyl)dimethylgermane

There total 2 articles about Chloro(chloromethyl)dimethylgermane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 917-54-4
methyllithium

: 21572-18-9
trichloro(chloromethyl)germane

: 5830-55-7
chloromethyltrimethylgermane

: 6727-63-5
Methylchlormethyldichlorgerman

: 6727-64-6
chloro(chloromethyl)dimethylgermane

Guidance literature:: In diethyl ether; (N2); dropwise addn. (1 h) of a soln. of methyllithium into the soln. of GeCl3CH2Cl at -70 °C under vigorous stirring; addnl. stirring (1.5 h); then standing the mixt. until room temp. was reached and addnl. stirring for 16 h;; filtration; then distg. the solvent off from the filtrate; vacuum distn.;
DOI:10.1016/0022-328X(88)87040-2

Reference yield:

: 6727-64-6
chloro(chloromethyl)dimethylgermane

Guidance literature:: Methylchlormethyldichlorgerman, Methyllithium; neben Chlormethyltrimethylgerman;

Reference yield: 89.0%

: 932-31-0
ortho-tolylmagnesium bromide

: 6727-64-6
chloro(chloromethyl)dimethylgermane

: 118165-90-5
chloromethyldimethyl(2-methylphenyl)germane

Guidance literature:: In tetrahydrofuran; under N2; after 3 h stirring at reflux reaction mixture quenched with satd. aq. NH4Cl; extraction with ether, concn., distn., elem. anal.;
DOI:10.1016/S0022-328X(00)99387-2