Chloromethylmethyldichlorogermane

Base Information

• Chemical Name: Chloromethylmethyldichlorogermane
• CAS No.: 6727-63-5
• Molecular Formula: C2H5Cl3Ge
• Molecular Weight: 208.06
• DSSTox Substance ID: DTXSID30700869
• Wikidata: Q82632353
• Mol file: 6727-63-5.mol

Synonyms:CHLOROMETHYLMETHYLDICHLOROGERMANE;6727-63-5;dichloro-(chloromethyl)-methylgermane;Dichloro(chloromethyl)methylgermane;DTXSID30700869

Chemical Property of Chloromethylmethyldichlorogermane

Chemical Property:

• Refractive Index: 1.492
• Boiling Point: 155°C
• PSA: 0.00000
• Density: 1,6694 g/cm3
• LogP: 2.73230
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 1
• Exact Mass: 207.866861
• Heavy Atom Count: 6
• Complexity: 44.1

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C[Ge](CCl)(Cl)Cl

Technology Process of Chloromethylmethyldichlorogermane

There total 1 articles about Chloromethylmethyldichlorogermane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methyllithium (917-54-4) + trichloro(chloromethyl)germane (21572-18-9) → chloromethyltrimethylgermane (5830-55-7) + Methylchlormethyldichlorgerman (6727-63-5) + chloro(chloromethyl)dimethylgermane (6727-64-6)

Guidance literature:

In diethyl ether; (N2); dropwise addn. (1 h) of a soln. of methyllithium into the soln. of GeCl3CH2Cl at -70 °C under vigorous stirring; addnl. stirring (1.5 h); then standing the mixt. until room temp. was reached and addnl. stirring for 16 h;; filtration; then distg. the solvent off from the filtrate; vacuum distn.;

DOI:10.1016/0022-328X(88)87040-2

upstream raw materials:

methyllithium

trichloro(chloromethyl)germane

Refernces