Benzenemethanol, 2-hydroxy-a-2-propenyl-

Base Information

• Chemical Name: Benzenemethanol, 2-hydroxy-a-2-propenyl-
• CAS No.: 67472-23-5
• Molecular Formula: C10H12O2
• Molecular Weight: 164.204
• Mol file: 67472-23-5.mol

Synonyms:1-(2-hydroxyphenyl)but-3-en-1-ol;2-(1-hydroxybut-3-enyl)phenol;1-(2-hydroxyphenyl)-3-buten-1-ol;2-(1-hydroxy-3-butenyl)phenol;1-(o-hydroxyphenyl)-3-buten-1-ol;2-(1'-hydroxybut-3'-enyl)phenol;

Chemical Property of Benzenemethanol, 2-hydroxy-a-2-propenyl-

Chemical Property:

• Boiling Point: 269.0±10.0 °C(Predicted)
• PSA: 40.46000
• Density: 1.116±0.06 g/cm3(Predicted)
• LogP: 2.00170

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Benzenemethanol, 2-hydroxy-a-2-propenyl-

There total 31 articles about Benzenemethanol, 2-hydroxy-a-2-propenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

2-methyl-benzyl alcohol (89-95-2) + allyltributylstanane (24850-33-7) → 2-(1-hydroxy-3-butenyl)phenol (67472-23-5)

Guidance literature:

With maleic acid; at 20 ℃; for 1.83333h;

DOI:10.1055/s-2005-917088

Reference yield: 99.0%

salicylaldehyde (90-02-8) + allyl bromide (106-95-6) → 2-(1-hydroxy-3-butenyl)phenol (67472-23-5)

Guidance literature:

With tin(ll) chloride; palladium dichloride; In water; at 20 ℃; for 24h;

DOI:10.1016/j.tet.2004.05.046

Reference yield: 99.0%

2-methyl-benzyl alcohol (89-95-2) + allyl bromide (106-95-6) → 2-(1-hydroxy-3-butenyl)phenol (67472-23-5)

Guidance literature:

With ammonium chloride; zinc; In tetrahydrofuran; water; at 20 ℃; for 0.133333h; sonication;

upstream raw materials:

trimethyl(allyl)stannane

salicylaldehyde

tetraallyl tin

allyl bromide