Ethyl 3-[dimethyl(phenyl)silyl]butanoate

Base Information

Chemical Name:Ethyl 3-[dimethyl(phenyl)silyl]butanoate
CAS No.:67473-43-2
Molecular Formula:C14H22O2Si
Molecular Weight:250.413
Hs Code.:
DSSTox Substance ID:DTXSID80508514
Nikkaji Number:J1.857.667H

Synonyms:Ethyl 3-[dimethyl(phenyl)silyl]butanoate;67473-43-2;DTXSID80508514

Suppliers and Price of Ethyl 3-[dimethyl(phenyl)silyl]butanoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of Ethyl 3-[dimethyl(phenyl)silyl]butanoate

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:6
Exact Mass:250.138906475
Heavy Atom Count:17
Complexity:245

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOC(=O)CC(C)[Si](C)(C)C1=CC=CC=C1

Technology Process of Ethyl 3-[dimethyl(phenyl)silyl]butanoate

There total 8 articles about Ethyl 3-[dimethyl(phenyl)silyl]butanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 3839-31-4
dimethyl(phenyl)silyllithium

: 623-70-1
ethyl (E)-crotonate

: 67473-43-2
3-(dimethyl(phenyl)silyl)butanoic acid ethyl ester

Guidance literature:: With copper(I) iodide dimethyl sulfide complex; In tetrahydrofuran; at -78 - 0 ℃; for 11h;
DOI:10.1021/jo048269e

Reference yield: 95.0%

: 3839-31-4
dimethyl(phenyl)silyl lithium

: 623-70-1
ethyl (E)-crotonate

: 67473-43-2
3-(dimethyl(phenyl)silyl)butanoic acid ethyl ester

Guidance literature:: dimethyl(phenyl)silyl lithium; With copper(I) iodide dimethyl sulfide complex; In tetrahydrofuran; at -78 ℃; for 0.5h;

ethyl (E)-crotonate; In tetrahydrofuran; at 0 ℃; for 8h; Further stages.;
DOI:10.1039/b210792a