Palladium, dichlorobis(4-methylpyridine)-

Base Information

Chemical Name:Palladium, dichlorobis(4-methylpyridine)-
CAS No.:67528-42-1
Molecular Formula:C₁₂H₁₄Cl₂N₂Pd
Molecular Weight:363.583
Hs Code.:

Synonyms:

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Chemical Property of Palladium, dichlorobis(4-methylpyridine)-

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of Palladium, dichlorobis(4-methylpyridine)-

There total 1 articles about Palladium, dichlorobis(4-methylpyridine)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 108-89-4
picoline

: 40691-28-9
PdCl₂(P(C₆H₅)(2-C₆H₄Cl)2)2

: 21256-09-7,67528-42-1
bis(4-methylpyridine)dichloridipalladium(II)

: 66185-98-6
bis-(2-chloro-phenyl)-phenyl-phosphane

Guidance literature:: In chloroform-d1; under N2; in NMR tube; 2 equiv. of ligand added to soln. of Pd complex in CDCl3; shaken for 2 min; not isolated; detd. by (31)P NMR spectra;
DOI:10.1021/om020885i

Reference yield: 43.0%

: 21256-09-7,67528-42-1
bis(4-methylpyridine)dichloridipalladium(II)

: HFe{Si(OSi(CH₃)3)3}(CO)3((C₆H₅)2PCH₂P(C₆H₅)2)

: (CO)3Fe(Si(OSi(CH₃)3)2(OSi(CH₃)3)((C₆H₅)2)PCH₂P(C₆H₅)2)PdCl

Guidance literature:: In dichloromethane; byproducts: 4-methylpyridine*HCl; (N2); Pd-compound was added to soln. of Fe-compound in CH2Cl2 at -25°C; soln. was warmed to room temp.; volatiles were removed in vac.; residue was extracted with warm Et2O-hexane (1:1); extract was filtered and slowly concd.; elem. anal.;

Reference yield: 30.0%

: 101-82-6
2-Benzylpyridine

: 21256-09-7,67528-42-1
bis(4-methylpyridine)dichloridipalladium(II)

: trans(N,N)-dichlorobis(4-methylpyridine)bis{μ-(pyridin-2-yl)phenylmethyl-N,C'}dipalladium(II) dichloromethane

: 28830-48-0
α,α'-bis-(2-pyridyl)bibenzyl

Guidance literature:: With n-C₄H₉Li; C₆H₆; CH₂Cl₂; In tetrahydrofuran; diethyl ether; 2-benzylpyridine deprotonated by n-C4H9Li in THF added to equimolar amt. of complex in Et2O at -80°C under N2, C6H6 added at room temp.,warmed at 60°C for 1 h, hydrolysed; extd. (hexane), recrystd. (CH2Cl2/acetone);
DOI:10.1016/S0020-1693(00)86742-0