2-Propen-1-one, 1-(4-chlorophenyl)-2-methyl-3,3-bis(methylthio)-

Base Information

Chemical Name:2-Propen-1-one, 1-(4-chlorophenyl)-2-methyl-3,3-bis(methylthio)-
CAS No.:67686-88-8
Molecular Formula:C12H13ClOS2
Molecular Weight:272.82
Hs Code.:
DSSTox Substance ID:DTXSID90454396
Nikkaji Number:J1.017.111C

Synonyms:67686-88-8;2-Propen-1-one, 1-(4-chlorophenyl)-2-methyl-3,3-bis(methylthio)-;DTXSID90454396;alpha-Methyl-beta,beta-bis(methylthio)-4'-chloroacrylophenone

Suppliers and Price of 2-Propen-1-one, 1-(4-chlorophenyl)-2-methyl-3,3-bis(methylthio)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 2-Propen-1-one, 1-(4-chlorophenyl)-2-methyl-3,3-bis(methylthio)-

Chemical Property:

XLogP3:4.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:4
Exact Mass:272.0096351
Heavy Atom Count:16
Complexity:275

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=C(SC)SC)C(=O)C1=CC=C(C=C1)Cl

Technology Process of 2-Propen-1-one, 1-(4-chlorophenyl)-2-methyl-3,3-bis(methylthio)-

There total 2 articles about 2-Propen-1-one, 1-(4-chlorophenyl)-2-methyl-3,3-bis(methylthio)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 67686-88-8
1-(4-chlorophenyl)-2-methyl-3,3-bis(methylthio)-prop-2-en-1-one

Guidance literature:: With iron(III) chloride; In N,N-dimethyl-formamide; at 120 ℃; for 20h; Schlenk technique; Inert atmosphere;

Reference yield: 56.0%

: 110-05-4
di-tert-butyl peroxide

: 41467-26-9
1-(4-chlorophenyl)-3,3-bis(methylsulfanyl)-2-propen-1-one

: 67686-88-8
1-(4-chlorophenyl)-2-methyl-3,3-bis(methylthio)-prop-2-en-1-one

Guidance literature:: With 1,4-diaza-bicyclo[2.2.2]octane; iron(III) chloride; In benzene; at 130 ℃; for 24h; Inert atmosphere; Sealed tube;
DOI:10.1002/adsc.201700654

Reference yield: 57.0%

: 67686-88-8
1-(4-chlorophenyl)-2-methyl-3,3-bis(methylthio)-prop-2-en-1-one

: 220278-19-3
2-bromo-2--p-chloropropiophenone

Guidance literature:: With pyridine; 1,3-dibromo-5,5-dimethylimidazolidine-2,4-dione; hydrogen fluoride; In dichloromethane; at -78 ℃; for 2h;
DOI:10.1016/S0040-4039(98)02191-1