Glycine, N-[N-[(1,1-dimethylethoxy)carbonyl]-D-alanyl]-, methyl ester

Base Information

Chemical Name:Glycine, N-[N-[(1,1-dimethylethoxy)carbonyl]-D-alanyl]-, methyl ester
CAS No.:67706-13-2
Molecular Formula:C11H20N2O5
Molecular Weight:260.29
Hs Code.:

Synonyms:Boc-Ala-Gly-OMe;Boc-L-alanine-glycine-OMe;methyl 2-((2S)-2-((tert-butoxycarbonyl)amino)propanamido)acetate;(S)-methyl 2-(2-(tert-butoxycarbonylamino)propanamido)acetate;Z-Ala-Gly-OMe;Boc-L-Ala-Gly-OMe;

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Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Glycine, N-[N-[(1,1-dimethylethoxy)carbonyl]-D-alanyl]-, methyl ester

Chemical Property:

PSA：93.73000
LogP:0.97060

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Glycine, N-[N-[(1,1-dimethylethoxy)carbonyl]-D-alanyl]-, methyl ester

There total 18 articles about Glycine, N-[N-[(1,1-dimethylethoxy)carbonyl]-D-alanyl]-, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 15761-38-3
L-N-Boc-Ala

: 5680-79-5,883886-67-7
glycine ethyl ester hydrochloride

: 26061-06-3,67706-13-2,28369-58-6
methyl 2-((2S)-2-((tert-butoxycarbonyl)amino)propanamido)acetate

Guidance literature:: With 4-methyl-morpholine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1016/j.fitote.2014.07.010

Reference yield: 99.0%

: 15761-38-3
L-N-Boc-Ala

: 616-34-2
methoxycarbonylmethylamine

: 26061-06-3,67706-13-2,28369-58-6
methyl 2-((2S)-2-((tert-butoxycarbonyl)amino)propanamido)acetate

Guidance literature:: L-N-Boc-Ala; With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; In N,N-dimethyl-formamide; at 20 ℃; for 0.333333h; Inert atmosphere;

methoxycarbonylmethylamine; With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 9h; Inert atmosphere;
DOI:10.1002/asia.201700339