(3S)-3-BOC-AMINO-1-DIAZO-4-METHYL-2-PENTANONE

Base Information

Chemical Name:(3S)-3-BOC-AMINO-1-DIAZO-4-METHYL-2-PENTANONE
CAS No.:67865-71-8
Molecular Formula:C11H19N3O3
Molecular Weight:241.28700
Hs Code.:
Mol file:67865-71-8.mol

Synonyms:(3S)-tert-butyl 3-diazo-1-isopropyl-2-oxopropylcarbamate;tert-butyl N-[(S)-1-diazenyl-1-isopropyl-2-oxopropyl]carbamate;(S)-3-(tert-butoxycarbonylamino)-1-diazo-4-methylpentan-2-one;Boc-Val-CH2N2;BOC-L-VAL-CHN2;Boc-L-valyl(diazo)methane;

Suppliers and Price of (3S)-3-BOC-AMINO-1-DIAZO-4-METHYL-2-PENTANONE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
(3S)-3-BOC-AMINO-1-DIAZO-4-METHYL-2-PENTANONE 95.00%
5MG
$ 501.79

American Custom Chemicals Corporation
(3S)-3-BOC-AMINO-1-DIAZO-4-METHYL-2-PENTANONE 95.00%
1G
$ 1155.00

Total 4 raw suppliers

Chemical Property of (3S)-3-BOC-AMINO-1-DIAZO-4-METHYL-2-PENTANONE

Chemical Property:

PSA：92.79000
LogP:1.87736

Purity/Quality:

99% ^*data from raw suppliers

(3S)-3-BOC-AMINO-1-DIAZO-4-METHYL-2-PENTANONE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of (3S)-3-BOC-AMINO-1-DIAZO-4-METHYL-2-PENTANONE

There total 9 articles about (3S)-3-BOC-AMINO-1-DIAZO-4-METHYL-2-PENTANONE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 186581-53-3,908094-01-9,334-88-3
diazomethane

: 13734-41-3
t-Boc-L-valine

: 67865-71-8
(S)-3-(tert-butoxycarbonylamino)-1-diazo-4-methylpentan-2-one

Guidance literature:: t-Boc-L-valine; With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; N,N-dimethyl-formamide; for 0.166667h;

diazomethane; In tetrahydrofuran; N,N-dimethyl-formamide; at 0 ℃; for 0.333333h;
DOI:10.1081/SCC-120023410

Reference yield: 69.0%

: 186581-53-3,908094-01-9,334-88-3
diazomethane

: 98807-40-0
Boc-Val-O-COOEt

: 67865-71-8
(S)-3-(tert-butoxycarbonylamino)-1-diazo-4-methylpentan-2-one

Guidance literature:: In diethyl ether; for 3h; Ambient temperature;

Reference yield: 31.0%

: 13734-41-3
t-Boc-L-valine

: 18107-18-1
diazomethyl-trimethyl-silane

: 67865-71-8
(S)-3-(tert-butoxycarbonylamino)-1-diazo-4-methylpentan-2-one

Guidance literature:: t-Boc-L-valine; With triethylamine; isobutyl chloroformate; In tetrahydrofuran; at 0 ℃; for 2h;

diazomethyl-trimethyl-silane; In tetrahydrofuran; hexane; acetonitrile; at 0 - 20 ℃; for 4h;