3-[(4-Methoxyphenyl)methyl]-4-methylpent-4-en-2-one

Base Information

Chemical Name:3-[(4-Methoxyphenyl)methyl]-4-methylpent-4-en-2-one
CAS No.:67935-55-1
Molecular Formula:C14H18O2
Molecular Weight:218.296
Hs Code.:
DSSTox Substance ID:DTXSID20527926

Synonyms:67935-55-1;3-[(4-Methoxyphenyl)methyl]-4-methylpent-4-en-2-one;SCHEMBL22923877;DTXSID20527926

Suppliers and Price of 3-[(4-Methoxyphenyl)methyl]-4-methylpent-4-en-2-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 3-[(4-Methoxyphenyl)methyl]-4-methylpent-4-en-2-one

Chemical Property:

XLogP3:3.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:5
Exact Mass:218.130679813
Heavy Atom Count:16
Complexity:250

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=C)C(CC1=CC=C(C=C1)OC)C(=O)C

Technology Process of 3-[(4-Methoxyphenyl)methyl]-4-methylpent-4-en-2-one

There total 1 articles about 3-[(4-Methoxyphenyl)methyl]-4-methylpent-4-en-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 141-79-7
4-methyl-pent-3-en-2-one

: 824-94-2
p-methoxybenzyl chloride

: 67935-55-1
2-Methyl-3-(4-methoxybenzyl)-4-oxo-1-penten

Guidance literature:: Multistep reaction; (i) NaNH₂, Fe(NO₃)3, liq. NH₃, (ii) /BRN= 606667/, Et₂O;
DOI:10.1055/s-1978-24833

Reference yield: 73.0%

: 67935-55-1
2-Methyl-3-(4-methoxybenzyl)-4-oxo-1-penten

: 89100-05-0
4-(4-Methoxy-phenyl)-3-(2-methyl-oxiranyl)-butan-2-one

Guidance literature:: With m-perbenzoic acid; In dichloromethane; for 12h;
DOI:10.1055/s-1983-30598

Reference yield:

: 67935-55-1
2-Methyl-3-(4-methoxybenzyl)-4-oxo-1-penten

: 89100-13-0
4-Hydroxy-2-(p-methoxybenzyl)-3-methyl-2-cyclopentenone

Guidance literature:: Multi-step reaction with 4 steps

1: 73 percent / m-perbenzoic acid / CH₂Cl₂ / 12 h

2: 64 percent / HCl / methanol / 6 h / 65 °C

3: 90 percent / tetraethylammonium perchlorate / 4 h / Ambient temperature; platinum foil electrodes (18.7 mA/cm²)

4: 2.) Na₂CO₃ / 1.) Amberllite 122 (acidic form) / 1.) dioxan, H₂O, r.t., 3 h, 2.) reflux, 6 h

With hydrogenchloride; m-perbenzoic acid; tetraethylammonium perchlorate; sodium carbonate; Amberllite 122 (acidic form); In methanol; dichloromethane;
DOI:10.1055/s-1983-30598