3-Methyl-3,4-dihydro-2H-1,5-benzodioxepin-3-ol

Base Information

Chemical Name:3-Methyl-3,4-dihydro-2H-1,5-benzodioxepin-3-ol
CAS No.:68281-26-5
Molecular Formula:C₁₀H₁₂O₃
Molecular Weight:180.203
Hs Code.:
ChEMBL ID:CHEMBL4591996
DSSTox Substance ID:DTXSID30505230
Wikidata:Q82360195

Synonyms:3-Methyl-3,4-dihydro-2H-1,5-benzodioxepin-3-ol;68281-26-5;3-METHYL-2,4-DIHYDRO-1,5-BENZODIOXEPIN-3-OL;3-hydroxy-3-methyl-2H-1,5-benzodioxepine;CHEMBL4591996;SCHEMBL11156161;DTXSID30505230;HWYICNJWLYVBPJ-UHFFFAOYSA-N;EN300-222844

Suppliers and Price of 3-Methyl-3,4-dihydro-2H-1,5-benzodioxepin-3-ol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of 3-Methyl-3,4-dihydro-2H-1,5-benzodioxepin-3-ol

Chemical Property:

XLogP3:1.5
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:0
Exact Mass:180.078644241
Heavy Atom Count:13
Complexity:165

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1(COC2=CC=CC=C2OC1)O

Technology Process of 3-Methyl-3,4-dihydro-2H-1,5-benzodioxepin-3-ol

There total 1 articles about 3-Methyl-3,4-dihydro-2H-1,5-benzodioxepin-3-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 598-09-4
2-chloromethyl-2-methyloxiran

: 120-80-9,19481-10-8,37349-32-9
benzene-1,2-diol

: 98-59-9
p-toluenesulfonyl chloride

: 68281-26-5
3,4-dihydro-3-methyl-2H-1,5-benzodioxepin-3-ol

: 16163-78-3
2,3-dihydro-2-methyl-1,4-benzodioxin-2-methyl 4-tolylsulfonate

Guidance literature:: With sodium hydroxide; Yield given. Multistep reaction; 1) 110 deg C, H₂O, 10 hrs., 2) pyridine, 5-10 deg C, 24 hrs.;
DOI:10.1002/jhet.5570170313