Ethyl 2-[(cyclohexyloxy)imino]-3-oxobutanoate

Base Information

Chemical Name:Ethyl 2-[(cyclohexyloxy)imino]-3-oxobutanoate
CAS No.:68401-41-2
Molecular Formula:C12H19NO4
Molecular Weight:241.287
Hs Code.:
DSSTox Substance ID:DTXSID70710760

Synonyms:Ethyl 2-[(cyclohexyloxy)imino]-3-oxobutanoate;68401-41-2;DTXSID70710760;UGHBGWAJKLJSLP-UHFFFAOYSA-N;ethyl 2-cyclohexyloxyimino-3-oxobutyrate

Suppliers and Price of Ethyl 2-[(cyclohexyloxy)imino]-3-oxobutanoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Ethyl 2-[(cyclohexyloxy)imino]-3-oxobutanoate

Chemical Property:

XLogP3:2.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:6
Exact Mass:241.13140809
Heavy Atom Count:17
Complexity:306

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOC(=O)C(=NOC1CCCCC1)C(=O)C

Technology Process of Ethyl 2-[(cyclohexyloxy)imino]-3-oxobutanoate

There total 4 articles about Ethyl 2-[(cyclohexyloxy)imino]-3-oxobutanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 108-85-0
1-bromocyclohexane

: 66508-93-8
ethyl 2-(hydroxyimino)-3-oxybutyrate

: 68401-41-2
ethyl (Z)-2-cyclohexyloxyimino-3-oxobutanoate

Guidance literature:: With potassium carbonate; In dimethyl sulfoxide; for 16h; Ambient temperature;
DOI:10.1039/P19910000881

Reference yield: 32.0%

: 66508-93-8
ethyl 2-(hydroxyimino)-3-oxybutyrate

: 1972-28-7,218603-74-8
diethylazodicarboxylate

: 68401-41-2
ethyl (Z)-2-cyclohexyloxyimino-3-oxobutanoate

Guidance literature:: With triphenylphosphine; In tetrahydrofuran; cyclohexanol;

Reference yield:

: 141-97-9
ethyl acetoacetate

: 68401-41-2
ethyl (Z)-2-cyclohexyloxyimino-3-oxobutanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / sodium nitrite, acetic acid / H₂O / 1 h / 0 deg C to r.t.

2: 63 percent / potassium carbonate / dimethylsulfoxide / 16 h / Ambient temperature

With potassium carbonate; acetic acid; sodium nitrite; In water; dimethyl sulfoxide;
DOI:10.1039/P19910000881