Benzeneethanol, b-cyclopropylidene-

Base Information

Chemical Name:Benzeneethanol, b-cyclopropylidene-
CAS No.:68423-19-8
Molecular Formula:C11H12O
Molecular Weight:160.216
Hs Code.:

Synonyms:2-Cyclopropylidene-2-phenyl-ethanol;2-cyclopropylidene-2-phenylethanol;2-Phenylcyclopropylidenethanol;cyclopropylidene-2-phenyl-1-ethanol;

Suppliers and Price of Benzeneethanol, b-cyclopropylidene-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of Benzeneethanol, b-cyclopropylidene-

Chemical Property:

Boiling Point:300.4±11.0 °C(Predicted)
PSA：20.23000
Density:1.157±0.06 g/cm3(Predicted)
LogP:2.22630

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Benzeneethanol, b-cyclopropylidene-

There total 4 articles about Benzeneethanol, b-cyclopropylidene- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 139198-68-8
tert-Butyl-(2-cyclopropylidene-2-phenyl-ethoxy)-diphenyl-silane

: 68423-19-8
2-cyclopropylidene-2-phenyl-1-ethanol

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; for 1.5h; Yield given; Ambient temperature;
DOI:10.1021/jo00032a021

Reference yield:

: 139167-15-0
2-(tert-butylphenylsilyloxy)acetophenone

: 68423-19-8
2-cyclopropylidene-2-phenyl-1-ethanol

Guidance literature:: Multi-step reaction with 2 steps

1: 1) NaH, 2) TDA-1 / 1) THF, 62 deg C, 10 h, 2) THF, 62 deg C, 1 h

2: n-Bu₄NF / tetrahydrofuran / 1.5 h / Ambient temperature

With tetrabutyl ammonium fluoride; sodium hydride; In tetrahydrofuran;
DOI:10.1021/jo00032a021

Reference yield:

: 582-24-1
1-phenyl-2-hydroxyethanone

: 68423-19-8
2-cyclopropylidene-2-phenyl-1-ethanol

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / imidazole, DMAP / dimethylformamide / 10 h / 0 °C

2: 1) NaH, 2) TDA-1 / 1) THF, 62 deg C, 10 h, 2) THF, 62 deg C, 1 h

3: n-Bu₄NF / tetrahydrofuran / 1.5 h / Ambient temperature

With 1H-imidazole; dmap; tetrabutyl ammonium fluoride; sodium hydride; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/jo00032a021