2-(4-Methoxyphenyl)-1,4-diphenylbutane-1,4-dione

Base Information

Chemical Name:2-(4-Methoxyphenyl)-1,4-diphenylbutane-1,4-dione
CAS No.:68614-52-8
Molecular Formula:C23H20O3
Molecular Weight:344.41
Hs Code.:
DSSTox Substance ID:DTXSID00497976
Nikkaji Number:J2.024.246I

Synonyms:2-(4-Methoxyphenyl)-1,4-diphenylbutane-1,4-dione;68614-52-8;DTXSID00497976

Suppliers and Price of 2-(4-Methoxyphenyl)-1,4-diphenylbutane-1,4-dione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 2-(4-Methoxyphenyl)-1,4-diphenylbutane-1,4-dione

Chemical Property:

XLogP3:4.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:7
Exact Mass:344.14124450
Heavy Atom Count:26
Complexity:452

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:COC1=CC=C(C=C1)C(CC(=O)C2=CC=CC=C2)C(=O)C3=CC=CC=C3

Technology Process of 2-(4-Methoxyphenyl)-1,4-diphenylbutane-1,4-dione

There total 7 articles about 2-(4-Methoxyphenyl)-1,4-diphenylbutane-1,4-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 637-69-4,24936-44-5
4-Methoxystyrene

: 17292-57-8
1-phenyl-1,2-propanedione-2-O-benzoyl oxime

: 100-52-7
benzaldehyde

: 68614-52-8
2-(p-methoxyphenyl)-1,4-diphenyl-1,4-butanedione

Guidance literature:: With 3-mesityl-4,5,6,7-tetrahydrobenzo[d]thiazol-3-ium perchlorate; N-ethyl-N,N-diisopropylamine; In acetonitrile; at 65 ℃; for 16h; regioselective reaction; Irradiation;
DOI:10.1021/acscatal.1c04594

Reference yield: 77.0%

: 5908-41-8
benzoyltrimethylsilane

: 22252-15-9
trans-4-methoxychalcone

: 68614-52-8
2-(p-methoxyphenyl)-1,4-diphenyl-1,4-butanedione

Guidance literature:: With 3-ethyl-5-(2-hydroxyethyl)-4-methyl-1,3-thiazolium bromide; 1,8-diazabicyclo[5.4.0]undec-7-ene; isopropyl alcohol; In tetrahydrofuran; at 70 ℃; for 24h;
DOI:10.1021/ja0318380

Reference yield: 74.0%

: 637-69-4,24936-44-5
4-Methoxystyrene

: diethyl 4-benzoyl-2,6-dimethyl-1,4-dihydropyridine-3,5-dicarboxylate

: 68614-52-8
2-(p-methoxyphenyl)-1,4-diphenyl-1,4-butanedione

Guidance literature:: With (1,2-dimethoxyethane)dichloronickel(II); In acetonitrile; at -78 ℃; for 48h; Inert atmosphere; Irradiation; Sealed tube;
DOI:10.1021/acs.orglett.9b04595