Germylene, diphenyl-

Base Information Edit

Chemical Name:Germylene, diphenyl-
CAS No.:68816-03-5
Molecular Formula:C12H10Ge
Molecular Weight:226.801
Hs Code.:
Mol file:68816-03-5.mol

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Germylene, diphenyl- Edit

Chemical Property:

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Technology Process of Germylene, diphenyl-

There total 20 articles about Germylene, diphenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: germanium(II) chloride dioxane

: 591-51-5
phenyllithium

: 68816-03-5
diphenylgermylene

Guidance literature:: In diethyl ether; hexane; byproducts: LiCl; the Ge-complex was suspensed in diethyl ether under Ar and cooled to 0°C; LiPh in hexane was added slowly within 15 min; stirred for 2 h; volatiles were evaporated; extraction with toluene; filtrated; toluene was evaporated under reduced pressure; elem. anal.;
DOI:10.1246/cl.1993.1385

Reference yield: 74.0%

: 1613-66-7
dichlorodiphenylgermane

: 68816-03-5
diphenylgermylene

Guidance literature:: With 15-crown-5; sodium; In diethyl ether; react. of germane with Na-sand in presence of 15-crown-5 in diethyl ether;
DOI:10.1039/c39900001147