Technology Process of Cyclononadecanone
There total 7 articles about Cyclononadecanone which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
trimethylsilyl iodide;
In
dichloromethane;
at 20 ℃;
for 21h;
Inert atmosphere;
DOI:10.1039/c3gc40905h
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1,2-bis{(di-tert-butylphosphino)methyl}benzene palladium ditriflate / 90 h / 90 °C / 15001.5 Torr / Glovebox; Schlenk technique; Inert atmosphere
2: sodium / 5,5-dimethyl-1,3-cyclohexadiene / 5 h / Inert atmosphere
3: trimethylsilyl iodide / dichloromethane / 21 h / 20 °C / Inert atmosphere
With
trimethylsilyl iodide; 1,2-bis{(di-tert-butylphosphino)methyl}benzene palladium ditriflate; sodium;
In
5,5-dimethyl-1,3-cyclohexadiene; dichloromethane;
DOI:10.1039/c3gc40905h
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium / 5,5-dimethyl-1,3-cyclohexadiene / 5 h / Inert atmosphere
2: trimethylsilyl iodide / dichloromethane / 21 h / 20 °C / Inert atmosphere
With
trimethylsilyl iodide; sodium;
In
5,5-dimethyl-1,3-cyclohexadiene; dichloromethane;
DOI:10.1039/c3gc40905h
