Carbamic acid, [[[(1,1-dimethylethoxy)carbonyl]amino][(2S)-2-[(1S,2S)-1-[[[(1,1-dimethyl ethyl)dimethylsilyl]oxy]methyl]-2-hydroxy-11-[(4-methoxyphenyl)methoxy] undecyl]-1-pyrrolidinyl]methylene]-, 1,1-dimethylethyl ester

Base Information

Chemical Name:Carbamic acid, [[[(1,1-dimethylethoxy)carbonyl]amino][(2S)-2-[(1S,2S)-1-[[[(1,1-dimethyl ethyl)dimethylsilyl]oxy]methyl]-2-hydroxy-11-[(4-methoxyphenyl)methoxy] undecyl]-1-pyrrolidinyl]methylene]-, 1,1-dimethylethyl ester
CAS No.:691006-75-4
Molecular Formula:C41H73N3O8Si
Molecular Weight:764.131
Hs Code.:

Carbamic acid,
[[[(1,1-dimethylethoxy)carbonyl]amino][(2S)-2-[(1S,2S)-1-[[[(1,1-dimethyl
ethyl)dimethylsilyl]oxy]methyl]-2-hydroxy-11-[(4-methoxyphenyl)methoxy]
undecyl]-1-pyrrolidinyl]methylene]-, 1,1-dimethylethyl ester

Synonyms:

Suppliers and Price of Carbamic acid, [[[(1,1-dimethylethoxy)carbonyl]amino][(2S)-2-[(1S,2S)-1-[[[(1,1-dimethyl ethyl)dimethylsilyl]oxy]methyl]-2-hydroxy-11-[(4-methoxyphenyl)methoxy] undecyl]-1-pyrrolidinyl]methylene]-, 1,1-dimethylethyl ester

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Chemical Property of Carbamic acid, [[[(1,1-dimethylethoxy)carbonyl]amino][(2S)-2-[(1S,2S)-1-[[[(1,1-dimethyl ethyl)dimethylsilyl]oxy]methyl]-2-hydroxy-11-[(4-methoxyphenyl)methoxy] undecyl]-1-pyrrolidinyl]methylene]-, 1,1-dimethylethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

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Hazard Codes:

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Useful:

Technology Process of Carbamic acid, [[[(1,1-dimethylethoxy)carbonyl]amino][(2S)-2-[(1S,2S)-1-[[[(1,1-dimethyl ethyl)dimethylsilyl]oxy]methyl]-2-hydroxy-11-[(4-methoxyphenyl)methoxy] undecyl]-1-pyrrolidinyl]methylene]-, 1,1-dimethylethyl ester

There total 10 articles about Carbamic acid, [[[(1,1-dimethylethoxy)carbonyl]amino][(2S)-2-[(1S,2S)-1-[[[(1,1-dimethyl ethyl)dimethylsilyl]oxy]methyl]-2-hydroxy-11-[(4-methoxyphenyl)methoxy] undecyl]-1-pyrrolidinyl]methylene]-, 1,1-dimethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (E)-12-(4-Methoxy-benzyloxy)-dodec-2-enoic acid ethyl ester

: 691006-75-4
(tert-butoxycarbonylimino-{2-[1-(tert-butyl-dimethyl-silanyloxymethyl)-2-hydroxy-11-(4-methoxy-benzyloxy)-undecyl]-pyrrolidin-1-yl}-methyl)-carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 8 steps

1: toluene / 19 h / 90 °C

2: LiAlH₄ / diethyl ether / 3 h / 0 °C

3: 6.63 g / CsF / ethanol / 13 h / 90 °C

4: 81 percent / pyridine / 19 h / 20 °C

5: 58 percent / DMAP; pyridine / 20 h / 20 °C

6: 94 percent / n-Bu₃SnH; AIBN / toluene / 0.5 h / 110 °C

7: H₂ / Pd(OH)2/C / ethanol / 3 h / 20 °C

8: 830 mg / HgCl₂; Et₃N / dimethylformamide / 0.5 h / 20 °C

With pyridine; dmap; lithium aluminium tetrahydride; 2,2'-azobis(isobutyronitrile); hydrogen; tri-n-butyl-tin hydride; triethylamine; cesium fluoride; mercury dichloride; palladium dihydroxide; In diethyl ether; ethanol; N,N-dimethyl-formamide; toluene;
DOI:10.1002/chem.200500852

Reference yield:

: 691006-74-3
3-(tert-butyl-dimethyl-silanyloxymethyl)-2-[9-(4-methoxy-benzyloxy)-nonyl]-hexahydro-pyrrolo[1,2-b]isoxazole

: 691006-75-4
(tert-butoxycarbonylimino-{2-[1-(tert-butyl-dimethyl-silanyloxymethyl)-2-hydroxy-11-(4-methoxy-benzyloxy)-undecyl]-pyrrolidin-1-yl}-methyl)-carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / Pd(OH)2/C / ethanol / 3 h / 20 °C

2: 830 mg / HgCl₂; Et₃N / dimethylformamide / 0.5 h / 20 °C

With hydrogen; triethylamine; mercury dichloride; palladium dihydroxide; In ethanol; N,N-dimethyl-formamide;
DOI:10.1002/chem.200500852

Reference yield:

: 691006-73-2
(2S,3S,3aR,4S)-3-Hydroxymethyl-2-[9-(4-methoxy-benzyloxy)-nonyl]-hexahydro-pyrrolo[1,2-b]isoxazol-4-ol

: 691006-75-4
(tert-butoxycarbonylimino-{2-[1-(tert-butyl-dimethyl-silanyloxymethyl)-2-hydroxy-11-(4-methoxy-benzyloxy)-undecyl]-pyrrolidin-1-yl}-methyl)-carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 81 percent / pyridine / 19 h / 20 °C

2: 58 percent / DMAP; pyridine / 20 h / 20 °C

3: 94 percent / n-Bu₃SnH; AIBN / toluene / 0.5 h / 110 °C

4: H₂ / Pd(OH)2/C / ethanol / 3 h / 20 °C

5: 830 mg / HgCl₂; Et₃N / dimethylformamide / 0.5 h / 20 °C

With pyridine; dmap; 2,2'-azobis(isobutyronitrile); hydrogen; tri-n-butyl-tin hydride; triethylamine; mercury dichloride; palladium dihydroxide; In ethanol; N,N-dimethyl-formamide; toluene;
DOI:10.1002/chem.200500852