5-Bromohex-5-en-1-ol

Base Information

Chemical Name:5-Bromohex-5-en-1-ol
CAS No.:69441-76-5
Molecular Formula:C6H11BrO
Molecular Weight:179.057
Hs Code.:
DSSTox Substance ID:DTXSID80498284
Wikidata:Q82348257

Synonyms:5-bromohex-5-en-1-ol;69441-76-5;5-bromo-hex-5-en-1-ol;SCHEMBL2352156;DTXSID80498284;CSTXIBXKUGBHJR-UHFFFAOYSA-N

Suppliers and Price of 5-Bromohex-5-en-1-ol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 5-Bromohex-5-en-1-ol

Chemical Property:

XLogP3:1.8
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:4
Exact Mass:177.99933
Heavy Atom Count:8
Complexity:70.9

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C=C(CCCCO)Br

Technology Process of 5-Bromohex-5-en-1-ol

There total 1 articles about 5-Bromohex-5-en-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 18343-91-4
5,6-dibromohexan-1-ol

: 928-90-5
5-hexyl-1-ol

: 69441-76-5
5-bromohex-5-en-1-ol

Guidance literature:: With potassium tert-butylate; In tert-butyl alcohol; at 40 ℃; for 24h; Reflux;

Reference yield:

: 69441-76-5
5-bromohex-5-en-1-ol

: 874-60-2
4-methyl-benzoyl chloride

: 455271-98-4
4-methyl-benzoic acid 5-bromo-hex-5-enyl ester

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 2h;

Reference yield:

: 69441-76-5
5-bromohex-5-en-1-ol

: C₁₆H₂₁BrO₂

Guidance literature:: Multi-step reaction with 2 steps

1: 1H-imidazole; triphenylphosphine; iodine / dichloromethane / 0 - 20 °C

2: FeBr₂(1,2-bis(diphenylphosphino)benzene); manganese; copper dichloride; lithium chloride / 1,2-dimethoxyethane / 15 h / 0 °C

With 1H-imidazole; manganese; FeBr₂(1,2-bis(diphenylphosphino)benzene); iodine; triphenylphosphine; lithium chloride; copper dichloride; In 1,2-dimethoxyethane; dichloromethane;
DOI:10.1021/acs.orglett.7b01128