2H-Pyrido[3,2-b]indol-2-one, 1,5-dihydro-1-[4-(5-isoxazolyl)phenyl]-5-methyl-

Base Information

Chemical Name:2H-Pyrido[3,2-b]indol-2-one, 1,5-dihydro-1-[4-(5-isoxazolyl)phenyl]-5-methyl-
CAS No.:698397-42-1
Molecular Formula:C21H15N3O2
Molecular Weight:341.369
Hs Code.:

Synonyms:

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Chemical Property of 2H-Pyrido[3,2-b]indol-2-one, 1,5-dihydro-1-[4-(5-isoxazolyl)phenyl]-5-methyl-

Chemical Property:

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Technology Process of 2H-Pyrido[3,2-b]indol-2-one, 1,5-dihydro-1-[4-(5-isoxazolyl)phenyl]-5-methyl-

There total 9 articles about 2H-Pyrido[3,2-b]indol-2-one, 1,5-dihydro-1-[4-(5-isoxazolyl)phenyl]-5-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 23.0%

: C₂₃H₂₁N₃O₂

: 698397-42-1
C₂₁H₁₅N₃O₂

Guidance literature:: With hydroxylamine hydrochloride; sodium acetate; In acetic acid; at 70 ℃;

Reference yield:

: 19012-02-3
N-methyl-3-acetylindole

: 698397-42-1
C₂₁H₁₅N₃O₂

Guidance literature:: Multi-step reaction with 8 steps

1.1: hydroxylamine; sodium acetate / ethanol; water / 2.5 h / Heating / reflux

2.1: acetic acid / 2 h / Heating / reflux

3.1: N,N-dimethyl-formamide; trichlorophosphate / 0.5 h / 0 °C

3.2: 0 - 20 °C

4.1: hydrogen; triethylamine / palladium 10% on activated carbon / tetrahydrofuran / 2 h

5.1: 3-chloro-benzenecarboperoxoic acid / ethanol / 2 h / Heating / reflux

5.2: 0.5 h / Heating / reflux

6.1: 4 A molecular sieve / copper diacetate / pyridine; DMF (N,N-dimethyl-formamide) / 80 h

7.1: acetonitrile / Heating / reflux

8.1: hydroxylamine; sodium acetate / acetic acid / 70 °C

With 4 A molecular sieve; hydrogen; hydroxylamine; sodium acetate; triethylamine; N,N-dimethyl-formamide; 3-chloro-benzenecarboperoxoic acid; trichlorophosphate; palladium 10% on activated carbon; copper diacetate; In tetrahydrofuran; pyridine; DMF (N,N-dimethyl-formamide); ethanol; water; acetic acid; acetonitrile;

Reference yield:

: 698397-51-2
C₁₂H₁₀N₂O

: 698397-42-1
C₂₁H₁₅N₃O₂

Guidance literature:: Multi-step reaction with 3 steps

1: 4 A molecular sieve / copper diacetate / pyridine; DMF (N,N-dimethyl-formamide) / 80 h

2: acetonitrile / Heating / reflux

3: hydroxylamine; sodium acetate / acetic acid / 70 °C

With 4 A molecular sieve; hydroxylamine; sodium acetate; copper diacetate; In pyridine; DMF (N,N-dimethyl-formamide); acetic acid; acetonitrile;